2-碘联苯

Mass

MS-NW-5428          
2-iodobiphenyl
C12H9I              (Mass of molecular ion:    280)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      39.0       2.9
      50.0       4.1
      51.0       5.6
      52.0       1.1
      61.0       1.1
      62.0       2.4
      63.0       5.4
      74.0       4.3
      75.0       5.1
      75.5       2.2
      76.0      12.1
      76.5       4.2
      77.0       4.8
      86.0       1.5
      87.0       2.0
      98.0       1.5
      99.0       1.3
     101.0       1.6
     102.0       1.8
     126.0       5.7
     127.0       4.8
     140.0       3.5
     150.0       4.3
     151.0      14.9
     152.0      57.9
     153.0      53.5
     154.0       7.3
     280.0     100.0
     281.0      13.4

Assign. Shift(ppm) A 7.934 B 7.55 to 7.18 C 7.003 J(A,C)=7.8HZ.

     Hz     ppm     Int.

    715.63   7.991    133
    715.13   7.985    138
    714.44   7.978    164
    713.88   7.971    145
    707.81   7.904    151
    707.19   7.897    159
    706.69   7.891    194
    706.06   7.884    165
    670.44   7.486     42
    668.44   7.464     72
    667.25   7.451     75
    665.88   7.436     62
    664.25   7.417     69
    662.50   7.398    191
    661.81   7.390    263
    660.81   7.379    403
    659.69   7.366   1000
    659.06   7.359    720
    658.19   7.350    673
    656.94   7.336    287
    655.88   7.324    316
    655.44   7.319    288
    654.56   7.309    381
    653.44   7.297    407
    653.13   7.293    412
    652.50   7.286    336
    650.94   7.269     62
    650.31   7.262     51
    649.88   7.257     72
    649.06   7.248     55
    648.31   7.239     83
    647.81   7.234     85
    646.31   7.217     30
    645.50   7.208     38
    644.81   7.200    111
    634.69   7.087    186
    631.88   7.056    129
    628.38   7.017    123
    626.88   7.000    154
    625.56   6.985    108
    623.94   6.967    108
    620.69   6.931    111
    617.75   6.898     92