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二苯基碘酰氯

产品名称 二苯基碘酰氯

CAS号1483-72-3

分子式C12H10ClI

分子量316.57

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  • Mass

    MS-NW-9113          
    diphenyliodonium chloride
    C12H10ClI           (Mass of molecular ion:    316)
    

       Source Temperature: 220 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          17.0       1.4
          18.0       7.4
          27.0       1.9
          36.0       4.2
          37.0       1.6
          38.0       4.7
          39.0       2.6
          49.0       2.0
          50.0      20.8
          51.0      32.5
          52.0       2.3
          56.0       1.6
          73.0       2.1
          74.0       7.4
          75.0       5.8
          76.0       6.3
          77.0     100.0
          78.0      10.1
         102.0       2.3
         112.0      41.2
         113.0       3.0
         114.0      14.9
         127.0       1.9
         154.0       2.2
         204.0      68.3
         205.0       4.3
         281.0       2.6
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C12 H10 Cl I 0.040 g : 0.5 ml DMSO-d6
    diphenyliodonium chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.118 B 7.556 C 7.438

         Hz     ppm     Int.
    

       3248.78   8.130    851
       3241.46   8.111    895
       3240.48   8.109    838
       3234.38   8.094     31
       3232.67   8.089     22
       3028.44   7.578    190
       3021.00   7.560    504
       3013.67   7.541    347
       2979.61   7.456    673
       2971.80   7.437   1000
       2965.94   7.422    195
       2964.23   7.418    473
    

in DMSO-d6



KBr disc



nujol mull