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网站主页CAS数据库列表 2001-45-8更多图谱四苯基氯化膦(2001-45-8)红外图谱(IR2)

四苯基氯化膦

产品名称 四苯基氯化膦

CAS号2001-45-8

分子式C24H20ClP

分子量374.84

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  • Mass

    MS-NW-7200          
    tetraphenylphosphonium chloride
    C24H20ClP           (Mass of molecular ion:    374)
    

       Source Temperature: 210 °C
       Sample Temperature: 260 °C
       Direct, 75 eV
    

          17.0       2.7
          18.0      11.7
          27.0       1.2
          28.0       1.4
          35.0       1.4
          36.0       9.1
          38.0       2.8
          39.0       4.0
          44.0       1.2
          50.0       3.8
          51.0       9.8
          52.0       2.7
          57.0       3.5
          63.0       2.5
          65.0       2.0
          74.0       1.6
          75.0       1.3
          76.0       1.9
          77.0       6.5
          78.0      10.4
          80.0       1.2
          81.0       2.7
          82.0       1.0
          83.0       1.5
          89.0       1.1
          91.0       1.2
         102.0       1.0
         107.0      14.9
         108.0      37.8
         109.0       3.5
         115.0       4.2
         128.0       1.7
         131.0       2.8
         133.0       3.6
         139.0       1.9
         141.0       1.7
         151.0       1.4
         152.0       9.0
         153.0       3.6
         154.0       5.1
         157.0       4.2
         170.0       3.0
         181.0       2.0
         182.0       1.2
         183.0      69.8
         184.0      15.6
         185.0      11.4
         186.0       1.9
         228.0       1.4
         230.0       1.2
         257.0       1.8
         259.0       3.0
         260.0       4.8
         261.0      19.1
         262.0     100.0
         263.0      19.6
         264.0       2.1
         337.0       4.3
         338.0       7.2
         339.0      10.0
         340.0       2.6
         414.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C24 H20 Cl P 0.033 g : 0.5 ml CDCl3
    tetraphenylphosphonium chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.953 B 7.832 C 7.644 J(P-31,A)=2.1HZ J(P-31,B)=3.7HZ J(P-31,C)=13.1HZ

         Hz     ppm     Int.
    

       3189.33   7.981    130
       3188.11   7.978    239
       3186.89   7.975    216
       3186.04   7.973    252
       3184.81   7.969    163
       3182.37   7.963    203
       3180.42   7.959    624
       3178.59   7.954    612
       3176.76   7.949    213
       3174.19   7.943    256
       3172.97   7.940    432
       3172.00   7.937    358
       3170.90   7.935    414
       3169.68   7.932    217
       3140.63   7.859    159
       3139.04   7.855    580
       3137.33   7.851    364
       3135.38   7.846    616
       3133.79   7.842    374
       3130.98   7.835   1000
       3129.03   7.830    559
       3127.32   7.826    955
       3125.98   7.822    376
       3123.41   7.816    545
       3121.70   7.812    307
       3119.75   7.807    494
       3067.14   7.675    185
       3065.43   7.671    776
       3064.21   7.668    901
       3063.23   7.665    452
       3058.96   7.655    273
       3057.01   7.650    830
       3055.66   7.646    683
       3054.20   7.643    248
       3052.37   7.638    784
       3051.27   7.635    903
       3050.29   7.633    455
       3045.90   7.622    268
       3043.95   7.617    806
       3042.72   7.614    649
    

in CDCl3



KBr disc



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