四苯基氯化膦

Mass

MS-NW-7200          
tetraphenylphosphonium chloride
C24H20ClP           (Mass of molecular ion:    374)

   Source Temperature: 210 °C
   Sample Temperature: 260 °C
   Direct, 75 eV

      17.0       2.7
      18.0      11.7
      27.0       1.2
      28.0       1.4
      35.0       1.4
      36.0       9.1
      38.0       2.8
      39.0       4.0
      44.0       1.2
      50.0       3.8
      51.0       9.8
      52.0       2.7
      57.0       3.5
      63.0       2.5
      65.0       2.0
      74.0       1.6
      75.0       1.3
      76.0       1.9
      77.0       6.5
      78.0      10.4
      80.0       1.2
      81.0       2.7
      82.0       1.0
      83.0       1.5
      89.0       1.1
      91.0       1.2
     102.0       1.0
     107.0      14.9
     108.0      37.8
     109.0       3.5
     115.0       4.2
     128.0       1.7
     131.0       2.8
     133.0       3.6
     139.0       1.9
     141.0       1.7
     151.0       1.4
     152.0       9.0
     153.0       3.6
     154.0       5.1
     157.0       4.2
     170.0       3.0
     181.0       2.0
     182.0       1.2
     183.0      69.8
     184.0      15.6
     185.0      11.4
     186.0       1.9
     228.0       1.4
     230.0       1.2
     257.0       1.8
     259.0       3.0
     260.0       4.8
     261.0      19.1
     262.0     100.0
     263.0      19.6
     264.0       2.1
     337.0       4.3
     338.0       7.2
     339.0      10.0
     340.0       2.6
     414.0       1.0

Assign. Shift(ppm) A 7.953 B 7.832 C 7.644 J(P-31,A)=2.1HZ J(P-31,B)=3.7HZ J(P-31,C)=13.1HZ

     Hz     ppm     Int.

   3189.33   7.981    130
   3188.11   7.978    239
   3186.89   7.975    216
   3186.04   7.973    252
   3184.81   7.969    163
   3182.37   7.963    203
   3180.42   7.959    624
   3178.59   7.954    612
   3176.76   7.949    213
   3174.19   7.943    256
   3172.97   7.940    432
   3172.00   7.937    358
   3170.90   7.935    414
   3169.68   7.932    217
   3140.63   7.859    159
   3139.04   7.855    580
   3137.33   7.851    364
   3135.38   7.846    616
   3133.79   7.842    374
   3130.98   7.835   1000
   3129.03   7.830    559
   3127.32   7.826    955
   3125.98   7.822    376
   3123.41   7.816    545
   3121.70   7.812    307
   3119.75   7.807    494
   3067.14   7.675    185
   3065.43   7.671    776
   3064.21   7.668    901
   3063.23   7.665    452
   3058.96   7.655    273
   3057.01   7.650    830
   3055.66   7.646    683
   3054.20   7.643    248
   3052.37   7.638    784
   3051.27   7.635    903
   3050.29   7.633    455
   3045.90   7.622    268
   3043.95   7.617    806
   3042.72   7.614    649