1,4-双(苯乙炔基)苯

产品名称 1,4-双(苯乙炔基)苯

CAS号1849-27-0

分子式C22H14

分子量278.35

¹³CNMR

Mass

MS-IW-5981          
p-bis(phenylethynyl)benzene
C22H14              (Mass of molecular ion:    278)

   Source Temperature: 160 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

     112.0       1.1
     113.0       2.1
     125.0       2.3
     126.0       1.2
     137.0       1.7
     138.0       4.7
     138.5       1.2
     139.0      15.1
     139.5       3.6
     250.0       1.4
     274.0       5.1
     275.0       3.0
     276.0      14.9
     277.0       3.9
     278.0     100.0
     279.0      24.0
     280.0       3.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₂₂ H₁₄	ca 1 mg : 0.5 ml CDCl₃
p-bis(phenylethynyl)benzene

    Assign.     Shift(ppm)

      A             7.54
      B             7.515
      C             7.36

     Hz     ppm     Int.

   3018.80   7.554    121
   3017.82   7.552     82
   3016.72   7.549     73
   3015.63   7.546     95
   3014.40   7.543    133
   3012.57   7.539     52
   3011.11   7.535    171
   3009.16   7.530    165
   3003.30   7.515   1000
   2948.73   7.379     61
   2947.39   7.375     39
   2946.41   7.373     47
   2944.70   7.369    161
   2942.87   7.364    187
   2939.82   7.356    279
   2937.74   7.351    309
   2935.30   7.345     39

in CDCl3

KBr disc

nujol mull

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1,4-双(苯乙炔基)苯(1849-27-0)核磁图(¹³CNMR) 相关产品图谱

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