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MassMS-NW-8024 1-chloro-9,10-bis(phenylethynyl)anthracene C30H17Cl (Mass of molecular ion: 412)
Source Temperature: 210 °C Sample Temperature: 180 °C Direct, 75 eV
18.0 1.1 148.0 1.4 149.0 1.8 150.0 1.0 154.5 1.1 160.0 1.4 161.0 3.6 161.5 1.7 162.0 3.7 162.5 1.0 166.5 1.0 167.0 1.0 167.5 2.3 168.0 1.0 168.5 1.0 173.0 3.0 173.5 1.6 174.0 5.4 174.5 1.8 175.0 3.8 175.5 1.2 180.5 1.7 185.0 1.1 186.0 5.4 186.5 2.7 187.0 15.6 187.5 7.0 188.0 6.4 188.5 1.9 206.0 22.3 206.5 7.3 207.0 8.4 207.5 2.6 298.0 1.8 299.0 1.0 300.0 3.7 301.0 1.0 322.0 1.0 346.0 1.2 348.0 2.0 350.0 1.9 372.0 4.9 373.0 2.5 374.0 16.3 375.0 7.9 376.0 13.9 377.0 4.7 378.0 3.2 379.0 1.1 410.0 1.6 411.0 1.1 412.0 100.0 413.0 33.9 414.0 37.8 415.0 11.2 416.0 1.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C30 H17 Cl 0.029 g : 0.5 ml CDCl3 1-chloro-9,10-bis(phenylethynyl)anthracene 
Assign. Shift(ppm)
A *1 8.833 B 8.621 C *1 8.589 D 7.72 E 7.61 F 7.42 G 7.39
Hz ppm Int.3538.82 8.855 34 3534.79 8.845 225 3532.71 8.840 234 3528.44 8.829 147 3525.27 8.821 255 3522.09 8.813 49 3450.56 8.634 332 3449.58 8.632 336 3441.89 8.613 360 3440.80 8.610 357 3436.89 8.600 254 3433.59 8.592 152 3429.57 8.582 241 3427.37 8.576 242 3423.46 8.567 42 3092.41 7.738 494 3088.62 7.729 711 3086.91 7.725 764 3084.59 7.719 742 3082.76 7.714 686 3080.57 7.709 681 3079.22 7.705 555 3076.78 7.699 125 3054.08 7.642 127 3049.44 7.631 585 3048.34 7.628 503 3045.41 7.621 375 3042.36 7.613 951 3039.18 7.605 388 3037.35 7.601 286 3035.64 7.596 288 3030.76 7.584 119 2979.49 7.456 128 2976.93 7.449 243 2975.71 7.446 300 2974.61 7.444 332 2973.14 7.440 276 2970.46 7.433 712 2968.51 7.428 882 2966.55 7.423 755 2964.23 7.418 986 2963.26 7.415 1000 2960.69 7.409 852 2958.62 7.404 934 2954.71 7.394 207 2951.42 7.386 567 2950.20 7.382 425 2942.87 7.364 297
in CDCl3
KBr disc
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