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MassMS-NW-8025 9,10-bis(phenylethynyl)anthracene C30H18 (Mass of molecular ion: 378)
Source Temperature: 220 °C Sample Temperature: 190 °C Direct, 75 eV
149.0 1.5 150.0 1.5 161.0 2.0 161.5 1.0 162.0 2.7 167.5 1.5 168.5 1.4 173.0 1.3 174.0 3.2 174.5 1.2 175.0 3.4 175.5 1.1 180.5 1.8 186.0 2.2 186.5 1.1 187.0 8.2 187.5 4.0 188.0 4.4 188.5 1.4 189.0 20.5 189.5 6.8 190.0 1.1 298.0 1.5 300.0 4.8 301.0 1.3 348.0 1.5 350.0 2.0 372.0 2.3 373.0 1.3 374.0 9.9 375.0 5.9 376.0 11.6 377.0 5.0 378.0 100.0 379.0 33.0 380.0 5.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C30 H18 saturated in CDCl3 9,10-bis(phenylethynyl)anthracene 
Assign. Shift(ppm)
A 8.700 B 7.784 C 7.645 D 7.462 E 7.43
Hz ppm Int.3485.72 8.722 83 3484.38 8.719 120 3481.69 8.712 909 3478.52 8.704 705 3475.10 8.696 678 3471.80 8.688 1000 3469.12 8.681 134 3467.77 8.678 94 3116.21 7.798 655 3114.62 7.794 630 3112.43 7.788 229 3109.74 7.782 337 3108.76 7.779 482 3108.03 7.777 803 3106.69 7.774 701 3104.25 7.768 95 3064.45 7.668 96 3063.11 7.665 129 3060.55 7.659 925 3057.25 7.650 647 3053.83 7.642 662 3050.54 7.634 894 3047.97 7.627 124 3046.63 7.624 86 2992.68 7.489 212 2991.09 7.485 163 2990.23 7.483 250 2988.65 7.479 136 2986.33 7.473 153 2983.89 7.467 748 2982.42 7.463 341 2981.32 7.460 236 2978.15 7.452 360 2976.56 7.448 736 2975.95 7.447 681 2974.00 7.442 654 2972.29 7.438 330 2970.09 7.432 164 2967.53 7.426 291 2966.80 7.424 284 2963.01 7.415 58 2961.18 7.410 66 2959.72 7.406 96 2958.25 7.403 43
in CDCl3
KBr disc
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