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网站主页CAS数据库列表 17337-13-2更多图谱异氰酸2-联苯酯(17337-13-2)核磁图(13CNMR)

异氰酸2-联苯酯

产品名称 异氰酸2-联苯酯

CAS号17337-13-2

分子式C13H9NO

分子量195.22

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  • Mass

    MS-IW-9296          
    2-biphenylyl isocyanate
    C13H9NO             (Mass of molecular ion:    195)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          28.0       1.5
          38.0       1.2
          39.0       4.4
          50.0       3.4
          51.0       5.7
          52.0       1.4
          62.0       2.8
          63.0       6.0
          64.0       1.6
          65.0       1.3
          69.0       2.5
          69.5       5.8
          70.0       3.3
          70.5       6.0
          74.0       2.3
          75.0       3.0
          76.0       2.6
          77.0       2.7
          82.5       3.0
          83.0       1.6
          83.5      16.3
          84.0       2.3
          86.0       1.2
          87.0       1.9
          88.0       2.2
          89.0       2.7
          97.5       1.8
         101.0       1.1
         102.0       1.2
         113.0       2.8
         114.0       2.6
         115.0       3.8
         126.0       1.1
         138.0       1.2
         139.0      13.3
         140.0      10.9
         141.0       1.8
         151.0       1.4
         152.0       1.9
         164.0       1.7
         165.0       1.6
         166.0      20.6
         167.0      65.4
         168.0       9.2
         194.0       1.2
         195.0     100.0
         196.0      14.7
         197.0       1.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H9 N O 0.05 ml : 0.5 ml CDCl3
    2-biphenylyl isocyanate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.41 B 7.38 C 7.36 D 7.282 E 7.232 F 7.193 G 7.115

         Hz     ppm     Int.
    

       2973.75   7.441    161
       2972.41   7.438    234
       2970.83   7.434    137
       2969.73   7.431     89
       2966.55   7.423    391
       2965.33   7.420    581
       2963.87   7.417    504
       2960.94   7.409    247
       2958.50   7.403    916
       2957.64   7.401    725
       2955.69   7.396    629
       2953.74   7.391   1000
       2953.13   7.390    871
       2950.44   7.383    209
       2948.24   7.378    473
       2946.90   7.374    596
       2945.68   7.371    286
       2944.95   7.369    275
       2944.21   7.367    180
       2942.50   7.363    208
       2940.92   7.359    204
       2939.82   7.356    389
       2936.52   7.348    102
       2935.06   7.345    114
       2932.98   7.339    148
       2915.89   7.297    263
       2915.41   7.295    277
       2913.94   7.292    319
       2913.33   7.290    291
       2908.45   7.278    423
       2906.62   7.273    445
       2906.13   7.272    417
       2900.63   7.258    170
       2898.68   7.254    175
       2893.19   7.240    470
       2891.24   7.235    352
       2885.62   7.221    482
       2883.54   7.216    368
       2881.10   7.210    412
       2879.39   7.205    463
       2873.66   7.191    439
       2872.19   7.187    378
       2866.21   7.172    172
       2864.75   7.169    135
       2848.39   7.128    395
       2847.90   7.126    404
       2846.56   7.123    400
       2840.82   7.109    284
       2840.21   7.107    307
       2839.11   7.104    287
       2838.62   7.103    262
    

in CDCl3



liquid film