顺-1,2-二氯乙烯

产品名称顺-1,2-二氯乙烯

CAS号156-59-2

分子式C2H2Cl2

分子量96.94

¹³CNMR

Mass

MS-NW-0847          
cis-1,2-dichloroethylene
C2H2Cl2             (Mass of molecular ion:     96)

   Source Temperature: 280 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       1.4
      24.0       1.1
      25.0       5.2
      26.0      13.9
      28.0       9.4
      32.0       2.6
      35.0       6.6
      36.0       2.0
      37.0       2.1
      47.0       6.3
      48.0       4.5
      49.0       2.9
      50.0       1.0
      59.0       1.8
      60.0      18.4
      61.0     100.0
      62.0       7.8
      63.0      32.0
      83.0      12.4
      85.0       8.3
      87.0       1.3
      95.0       1.7
      96.0      83.4
      97.0       2.8
      98.0      53.3
      99.0       1.2
     100.0       8.6

parameter in TMS

parameter in CDCl3

¹H NMR	300 MHz
C₂ H₂ Cl₂	5 % in TMS
cis-1,2-dichloroethylene

    Parameter     ppm  Hz

      D(A)         6.278
      D(B)         6.278
       J(A,B)          5.3
     
     WHIPPLE,E.B. ET AL. J.CHEM.PHYS. 34, 2136 (1961)

     Hz     ppm     Int.

   1883.40   6.278   1000

¹H NMR	300 MHz
C₂ H₂ Cl₂	0.04 ml : 0.5 ml CDCl₃
cis-1,2-dichloroethylene

    Parameter     ppm  Hz

      D(A)         6.421

     Hz     ppm     Int.

   1926.30   6.421   1000

in CDCl3

liquid film

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