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顺-1,2-二氯乙烯

产品名称 顺-1,2-二氯乙烯

CAS号156-59-2

分子式C2H2Cl2

分子量96.94

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  • Mass

    MS-NW-0847          
    cis-1,2-dichloroethylene
    C2H2Cl2             (Mass of molecular ion:     96)
    

       Source Temperature: 280 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       1.4
          24.0       1.1
          25.0       5.2
          26.0      13.9
          28.0       9.4
          32.0       2.6
          35.0       6.6
          36.0       2.0
          37.0       2.1
          47.0       6.3
          48.0       4.5
          49.0       2.9
          50.0       1.0
          59.0       1.8
          60.0      18.4
          61.0     100.0
          62.0       7.8
          63.0      32.0
          83.0      12.4
          85.0       8.3
          87.0       1.3
          95.0       1.7
          96.0      83.4
          97.0       2.8
          98.0      53.3
          99.0       1.2
         100.0       8.6
    

parameter in TMS

parameter in CDCl3


  • 1H NMR 300 MHz
    C2 H2 Cl2 5 % in TMS
    cis-1,2-dichloroethylene
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 6.278 D(B) 6.278 J(A,B) 5.3 WHIPPLE,E.B. ET AL. J.CHEM.PHYS. 34, 2136 (1961)

         Hz     ppm     Int.
    

       1883.40   6.278   1000
    


  • 1H NMR 300 MHz
    C2 H2 Cl2 0.04 ml : 0.5 ml CDCl3
    cis-1,2-dichloroethylene
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 6.421

         Hz     ppm     Int.
    

       1926.30   6.421   1000
    

in CDCl3



liquid film