1-氰基哌啶

Mass

MS-NW-8577          
1-piperidinecarbonitrile
C6H10N2             (Mass of molecular ion:    110)

   Source Temperature: 250 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      15.0       2.5
      26.0       3.0
      27.0      15.6
      28.0      24.9
      29.0      10.9
      30.0       1.9
      38.0       1.2
      39.0      16.2
      40.0       4.0
      41.0      45.2
      42.0     100.0
      43.0      27.7
      44.0       2.8
      51.0       1.5
      52.0       1.2
      53.0      10.6
      54.0      13.2
      55.0      48.6
      56.0      13.8
      57.0      22.3
      65.0       1.5
      67.0      11.2
      68.0       6.8
      69.0      56.1
      70.0       4.4
      81.0       3.8
      82.0       9.6
      83.0       3.5
      92.0       2.2
      95.0       4.6
     109.0      53.7
     110.0      73.8
     111.0       9.3

Assign. Shift(ppm) A 3.19 B 1.68 C 1.61

     Hz     ppm     Int.

    295.81   3.303     38
    295.31   3.298     45
    287.81   3.214    431
    285.50   3.188    612
    280.00   3.127    461
    273.69   3.056     45
    272.69   3.045     37
    162.44   1.814     39
    161.31   1.802     44
    158.88   1.775     77
    157.81   1.763     78
    156.25   1.745     99
    152.88   1.708    262
    149.69   1.672    426
    146.56   1.637    800
    145.31   1.623   1000
    143.75   1.606    940
    141.94   1.585    818
    134.63   1.504     64
    134.31   1.500     59
    132.63   1.481     40
    132.06   1.475     38
    131.38   1.467     37