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MS-NW-6429 ethyl 2-pyridinecarboxylate C8H9NO2 (Mass of molecular ion: 151)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
26.0 2.1 27.0 8.1 28.0 2.2 29.0 13.0 39.0 1.9 50.0 3.9 51.0 15.3 52.0 10.7 53.0 1.1 76.0 1.2 77.0 1.4 78.0 47.4 79.0 100.0 80.0 9.2 106.0 15.7 107.0 21.5 108.0 1.5 151.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H9 N O2 0.05 ml : 0.5 ml CDCl3 ethyl 2-pyridinecarboxylate Assign. Shift(ppm)
A 8.771 B 8.146 C 7.864 D 7.496 E 4.492 F 1.454
Hz ppm Int.
3509.28 8.781 131 3508.30 8.779 143 3507.45 8.777 144 3506.59 8.775 133 3504.52 8.769 135 3503.66 8.767 146 3502.81 8.765 142 3501.83 8.763 129 3260.99 8.160 143 3260.01 8.158 205 3258.91 8.155 136 3253.17 8.141 162 3252.08 8.138 229 3251.10 8.135 154 3151.49 7.886 129 3149.78 7.882 127 3143.80 7.867 227 3142.09 7.863 219 3135.99 7.847 125 3134.28 7.843 122 3002.56 7.513 141 3001.34 7.510 140 2997.80 7.502 141 2996.58 7.499 142 2994.87 7.494 133 2993.65 7.491 127 2990.11 7.482 127 2988.89 7.479 122 1806.15 4.520 211 1799.07 4.502 575 1791.87 4.484 572 1784.79 4.466 214 588.26 1.472 597 585.69 1.466 31 581.05 1.454 1000 573.85 1.436 573
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