4-氰基-4-苯基哌嗪

Mass

MS-NW-8209          
4-phenyl-4-piperidinecarbonitrile hydrochloride
C12H14N2 HCl        (Mass of molecular ion:    186)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

      27.0       3.7
      28.0      17.1
      29.0      13.1
      30.0      12.3
      35.0       3.5
      36.0      22.3
      37.0       1.2
      38.0       7.7
      39.0       4.0
      41.0       2.3
      42.0      12.5
      43.0      90.4
      44.0       5.8
      50.0       2.5
      51.0       7.4
      52.0       2.5
      53.0       4.1
      54.0       1.7
      55.0       1.6
      56.0      81.7
      57.0     100.0
      58.0       3.8
      62.0       1.0
      63.0       3.2
      64.0       1.2
      65.0       2.7
      68.0       2.2
      69.0       2.3
      74.0       1.0
      75.0       1.8
      76.0       2.6
      77.0       9.1
      78.0       3.7
      79.0       1.0
      80.0       1.9
      82.0       2.1
      89.0       2.7
      91.0       9.8
      92.0       2.5
      93.0       1.0
      95.0       6.1
     101.0       1.5
     102.0       4.9
     103.0       6.6
     104.0       1.6
     105.0       2.0
     106.0       3.0
     107.0       2.3
     108.0      12.1
     109.0       2.7
     115.0       8.0
     116.0       3.8
     117.0       1.9
     118.0       1.1
     119.0       2.9
     127.0       2.0
     128.0       5.2
     129.0       8.0
     130.0       4.5
     131.0       1.2
     140.0       1.7
     142.0       1.0
     143.0       1.9
     144.0       1.2
     154.0       1.0
     155.0       2.6
     156.0       1.4
     157.0       1.1
     158.0       4.5
     159.0       9.4
     160.0       1.3
     185.0      16.2
     186.0      88.0
     187.0      12.9

Assign. Shift(ppm) A 9.71 B 7.560 C 7.510 D 7.437 E 3.51 F 3.102 G 2.51 J 2.376 SIGNAL E OVERLAPPED BY H2O SIGNAL G OVERLAPPED BY SOLVENT

     Hz     ppm     Int.

   3879.85   9.709    136
   3027.80   7.577    389
   3026.28   7.573    548
   3018.34   7.553   1000
   3008.42   7.528    579
   3001.10   7.510    852
   2993.16   7.490    436
   2986.76   7.474     32
   2986.30   7.473     31
   2985.53   7.471     30
   2984.62   7.469     31
   2982.94   7.464     34
   2982.33   7.463     33
   2980.80   7.459     37
   2976.07   7.447    351
   2974.85   7.444    238
   2971.04   7.435    169
   2968.90   7.429    416
   2961.88   7.412    150
   1410.22   3.529    360
   1396.64   3.495    477
   1251.68   3.132    235
   1240.54   3.105    391
   1238.56   3.100    408
   1227.57   3.072    219
   1225.59   3.067    204
   1019.90   2.552    164
   1015.32   2.541    229
   1005.86   2.517    373
   1002.66   2.509    345
    992.58   2.484    253
    988.92   2.475    220
    955.20   2.391    507
    941.16   2.355    325