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网站主页CAS数据库列表 1499-21-4更多图谱二苯基次膦酰氯(1499-21-4)核磁图(1HNMR)

二苯基次膦酰氯

产品名称 二苯基次膦酰氯

CAS号1499-21-4

分子式C12H10ClOP

分子量236.63

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  • Mass

    MS-IW-8116          
    diphenylphosphinic chloride
    C12H10ClOP          (Mass of molecular ion:    236)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          39.0       1.0
          47.0       3.0
          50.0       3.5
          51.0      13.9
          74.0       1.3
          75.0       1.4
          76.0       2.9
          77.0      25.1
          78.0       2.2
          95.0       1.3
          99.5       2.8
         100.0       1.8
         107.0       3.2
         123.0       1.0
         128.0       1.0
         143.0      14.7
         144.0       1.0
         145.0       4.9
         151.0       1.7
         152.0       8.6
         153.0       4.1
         154.0       3.1
         159.0       1.8
         170.0       1.1
         171.0       1.6
         173.0       2.0
         183.0       4.0
         199.0      40.8
         200.0       9.9
         201.0      46.4
         202.0       6.1
         219.0       1.6
         235.0     100.0
         236.0      50.1
         237.0      39.4
         238.0      16.6
         239.0       2.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H10 Cl O P 0.05 ml : 0.5 ml CDCl3
    diphenylphosphinic chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.867 B 7.567 C 7.491

         Hz     ppm     Int.
    

       3157.96   7.902    140
       3156.25   7.898    608
       3154.91   7.895    820
       3153.44   7.891    426
       3150.02   7.882    267
       3147.95   7.877   1000
       3146.48   7.874    836
       3143.68   7.867    155
       3141.85   7.862    630
       3140.50   7.859    852
       3139.16   7.855    424
       3135.62   7.846    261
       3133.54   7.841    998
       3132.08   7.838    841
       3035.40   7.596    116
       3034.18   7.593    219
       3033.57   7.591    179
       3032.23   7.588    253
       3030.88   7.584    165
       3029.05   7.580    170
       3026.98   7.575    516
       3024.54   7.568    555
       3022.58   7.564    224
       3020.63   7.559    301
       3019.29   7.555    512
       3018.68   7.554    407
       3017.33   7.550    535
       3015.99   7.547    277
       3012.08   7.537     45
       3010.99   7.535     43
       3005.86   7.522     80
       3004.27   7.518    195
       3003.17   7.515    487
       3002.44   7.513    665
       3001.10   7.510    380
       3000.00   7.507    258
       2998.90   7.504    518
       2998.17   7.502    686
       2996.22   7.498    638
       2994.75   7.494    960
       2993.16   7.490    381
       2991.82   7.487    559
       2990.48   7.483    956
       2989.14   7.480    469
       2987.67   7.476    523
       2986.45   7.473    349
       2984.86   7.469    234
       2983.28   7.465    450
       2982.30   7.463    314
    

in CDCl3



liquid film