二苯基次膦酰氯

产品名称二苯基次膦酰氯

CAS号1499-21-4

分子式C12H10ClOP

分子量236.63

¹³CNMR

Mass

MS-IW-8116          
diphenylphosphinic chloride
C12H10ClOP          (Mass of molecular ion:    236)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      39.0       1.0
      47.0       3.0
      50.0       3.5
      51.0      13.9
      74.0       1.3
      75.0       1.4
      76.0       2.9
      77.0      25.1
      78.0       2.2
      95.0       1.3
      99.5       2.8
     100.0       1.8
     107.0       3.2
     123.0       1.0
     128.0       1.0
     143.0      14.7
     144.0       1.0
     145.0       4.9
     151.0       1.7
     152.0       8.6
     153.0       4.1
     154.0       3.1
     159.0       1.8
     170.0       1.1
     171.0       1.6
     173.0       2.0
     183.0       4.0
     199.0      40.8
     200.0       9.9
     201.0      46.4
     202.0       6.1
     219.0       1.6
     235.0     100.0
     236.0      50.1
     237.0      39.4
     238.0      16.6
     239.0       2.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₁₀ Cl O P	0.05 ml : 0.5 ml CDCl₃
diphenylphosphinic chloride

    Assign.     Shift(ppm)

      A             7.867
      B             7.567
      C             7.491

     Hz     ppm     Int.

   3157.96   7.902    140
   3156.25   7.898    608
   3154.91   7.895    820
   3153.44   7.891    426
   3150.02   7.882    267
   3147.95   7.877   1000
   3146.48   7.874    836
   3143.68   7.867    155
   3141.85   7.862    630
   3140.50   7.859    852
   3139.16   7.855    424
   3135.62   7.846    261
   3133.54   7.841    998
   3132.08   7.838    841
   3035.40   7.596    116
   3034.18   7.593    219
   3033.57   7.591    179
   3032.23   7.588    253
   3030.88   7.584    165
   3029.05   7.580    170
   3026.98   7.575    516
   3024.54   7.568    555
   3022.58   7.564    224
   3020.63   7.559    301
   3019.29   7.555    512
   3018.68   7.554    407
   3017.33   7.550    535
   3015.99   7.547    277
   3012.08   7.537     45
   3010.99   7.535     43
   3005.86   7.522     80
   3004.27   7.518    195
   3003.17   7.515    487
   3002.44   7.513    665
   3001.10   7.510    380
   3000.00   7.507    258
   2998.90   7.504    518
   2998.17   7.502    686
   2996.22   7.498    638
   2994.75   7.494    960
   2993.16   7.490    381
   2991.82   7.487    559
   2990.48   7.483    956
   2989.14   7.480    469
   2987.67   7.476    523
   2986.45   7.473    349
   2984.86   7.469    234
   2983.28   7.465    450
   2982.30   7.463    314

in CDCl3

liquid film

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二苯基次膦酰氯(1499-21-4)核磁图(¹HNMR) 相关产品图谱

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