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MS-IW-1779 4,4'-(hexafluoroisopropylidene)dianiline C15H12F6N2 (Mass of molecular ion: 334)
Source Temperature: 140 °C Sample Temperature: 110 °C Direct, 75 eV
28.0 1.0 65.0 1.4 83.5 2.5 84.0 1.0 97.5 4.9 98.0 13.9 98.5 2.1 132.5 9.0 133.0 1.6 142.0 1.3 152.0 1.0 167.0 3.9 168.0 2.3 179.0 1.7 180.0 4.4 195.0 14.1 196.0 7.2 197.0 1.0 198.0 2.8 225.0 1.8 244.0 1.0 246.0 1.1 248.0 1.8 249.0 1.6 263.0 1.4 264.0 7.7 265.0 100.0 266.0 15.9 267.0 1.2 315.0 3.3 333.0 3.1 334.0 73.3 335.0 12.5
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C15 H12 F6 N2 0.038 g : 0.5 ml DMSO-d6 4,4'-(hexafluoroisopropylidene)dianiline Assign. Shift(ppm)
A 6.967 B 6.573 C 5.41
Hz ppm Int.
2789.06 6.979 513 2780.64 6.958 580 2769.90 6.931 25 2769.04 6.929 23 2768.68 6.928 23 2768.07 6.927 22 2631.47 6.585 887 2622.56 6.563 821 2613.28 6.539 25 2612.67 6.538 23 2612.06 6.536 23 2610.60 6.533 22 2161.38 5.409 1000
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