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MassMS-IW-1309 1-(2-(p-bromophenoxy)ethyl)pyrrolidine C12H16BrNO (Mass of molecular ion: 269)
Source Temperature: 230 °C Sample Temperature: 160 °C Reservoir, 75 eV
28.0 1.0 30.0 1.2 41.0 2.0 42.0 6.6 55.0 3.5 56.0 2.9 69.0 1.4 82.0 1.3 84.0 100.0 85.0 6.1 96.0 1.2 97.0 1.2 98.0 1.1 269.0 1.5 271.0 1.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C12 H16 Br N O 0.05 ml : 0.5 ml CDCl3 1-(2-(p-bromophenoxy)ethyl)pyrrolidine 
Assign. Shift(ppm)
A 7.335 B 6.783 C 4.042 D 2.866 E 2.60 F 1.783
Hz ppm Int.665.56 7.432 83 664.75 7.423 57 662.31 7.396 684 660.00 7.370 244 658.31 7.351 71 657.75 7.345 75 655.50 7.320 290 653.19 7.294 1000 649.94 7.258 135 614.75 6.865 113 611.50 6.828 858 609.19 6.803 259 604.63 6.752 222 602.38 6.726 611 599.19 6.691 81 368.31 4.113 361 365.94 4.086 73 362.38 4.047 806 359.69 4.017 71 356.50 3.981 442 262.31 2.929 453 260.19 2.906 80 256.50 2.865 825 253.25 2.828 91 250.50 2.798 378 246.50 2.753 49 245.94 2.747 48 245.56 2.742 48 243.88 2.724 59 243.00 2.714 62 242.13 2.704 67 239.94 2.680 184 239.13 2.671 222 237.75 2.655 253 237.00 2.647 251 235.44 2.629 323 232.75 2.599 670 230.63 2.576 468 228.81 2.555 333 227.25 2.538 345 226.13 2.525 372 223.44 2.495 117 219.81 2.455 61 174.56 1.950 44 169.50 1.893 74 166.50 1.860 314 163.44 1.825 405 159.75 1.784 782 156.25 1.745 423 153.19 1.711 260 150.31 1.679 83
in CDCl3
liquid film
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