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网站主页CAS数据库列表 101-96-2更多图谱N,N'-二仲丁基对苯二胺(101-96-2)核磁图(1HNMR)

N,N'-二仲丁基对苯二胺

产品名称 N,N'-二仲丁基对苯二胺

CAS号101-96-2

分子式C14H24N2

分子量220.35

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  • Mass

    MS-IW-5650          
    N,N'-di-sec-butyl-p-phenylenediamine
    C14H24N2            (Mass of molecular ion:    220)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       1.1
          28.0       1.4
          29.0       3.4
          39.0       1.4
          41.0       3.5
          42.0       1.2
          53.0       1.0
          57.0       1.7
          65.0       2.0
          73.0       1.1
          74.0       3.3
          77.0       1.1
          79.0       1.3
          80.0       4.3
          81.0      13.9
          81.5       1.6
          88.0       2.0
          91.0       1.8
          92.0       1.9
          93.0       2.2
         106.0       2.1
         107.0      14.9
         108.0       2.4
         117.0       1.2
         118.0       4.8
         119.0       5.0
         120.0       9.8
         121.0       1.0
         132.0       1.5
         133.0       3.4
         134.0       3.3
         135.0       4.8
         147.0       2.0
         161.0       6.6
         162.0       1.6
         163.0       7.3
         164.0       1.7
         175.0       2.5
         189.0       4.9
         190.0       2.2
         191.0     100.0
         192.0      14.1
         205.0      13.7
         206.0       2.1
         218.0       1.6
         219.0       3.2
         220.0      37.5
         221.0       6.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H24 N2 0.05 ml : 0.5 ml CDCl3
    N,N'-di-sec-butyl-p-phenylenediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.514 B 3.259 C 2.96 D *1 1.580 E *1 1.404 F 1.123 G 0.928

         Hz     ppm     Int.
    

       2603.76   6.516    962
       1312.13   3.284     58
       1305.91   3.268    101
       1299.93   3.253    103
       1293.70   3.238     62
       1181.64   2.957     76
        646.12   1.617     52
        640.63   1.603     66
        638.67   1.599     61
        634.64   1.588     43
        632.93   1.584     98
        627.20   1.570     80
        625.12   1.565     84
        619.75   1.551     74
        617.68   1.546     33
        574.34   1.438     85
        567.14   1.420    127
        560.55   1.403     99
        559.94   1.402    109
        553.59   1.386     92
        546.39   1.368     66
        452.03   1.132   1000
        445.80   1.116    976
        442.02   1.107     43
        382.20   0.957     36
        378.30   0.947    505
        370.85   0.928    932
        363.40   0.910    435
    

in CDCl3



liquid film