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MassMS-NW-4813 1,1-dimethoxycyclohexane C8H16O2 (Mass of molecular ion: 144)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
14.0 1.8 15.0 17.0 18.0 3.5 26.0 2.7 27.0 25.3 28.0 7.0 29.0 20.4 30.0 3.3 31.0 40.9 32.0 27.0 38.0 2.7 39.0 35.7 40.0 5.9 41.0 56.8 42.0 5.2 43.0 78.6 44.0 2.0 45.0 26.3 50.0 3.0 51.0 5.5 52.0 3.5 53.0 14.0 54.0 28.3 55.0 20.4 56.0 2.3 57.0 4.9 58.0 9.9 59.0 2.5 65.0 3.5 66.0 2.6 67.0 11.4 68.0 2.9 69.0 14.0 70.0 1.2 71.0 9.1 72.0 1.7 77.0 8.0 78.0 1.7 79.0 18.4 80.0 5.2 81.0 43.5 82.0 4.3 83.0 17.7 84.0 87.3 85.0 5.5 88.0 9.8 95.0 1.0 96.0 1.4 97.0 45.0 98.0 3.5 101.0 100.0 102.0 7.4 109.0 1.1 111.0 49.1 112.0 62.7 113.0 51.9 114.0 4.1 115.0 3.4 144.0 6.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H16 O2 0.04 ml : 0.5 ml CDCl3 1,1-dimethoxycyclohexane 
Assign. Shift(ppm)
A 3.177 B 1.633 C 1.501 D 1.41
Hz ppm Int.1269.78 3.178 1000 658.33 1.648 43 652.95 1.634 66 646.48 1.618 59 611.33 1.530 25 605.83 1.516 41 599.85 1.501 61 594.12 1.487 40 588.26 1.472 21 564.33 1.413 28 559.20 1.400 29
in CDCl3
CCl4 solution
liquid film
4880 A,200 M,liquid
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