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1,4-Dioxaspiro[4.5]decan-8-one

Product Name 1,4-Dioxaspiro[4.5]decan-8-one

CAS4746-97-8

MFC8H12O3

MW156.18

¹³CNMR

Mass

MS-IW-4170          
1,4-dioxaspiro(4.5)decan-8-one
C8H12O3             (Mass of molecular ion:    156)

   Source Temperature: 240 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       3.1
      28.0       5.6
      29.0       1.5
      39.0       1.8
      41.0       2.0
      42.0       2.9
      43.0       3.4
      45.0       1.4
      53.0       1.1
      54.0       1.9
      55.0      13.5
      56.0       9.0
      57.0       2.2
      67.0       2.6
      71.0       1.7
      83.0       2.4
      84.0       4.0
      86.0       4.0
      97.0       2.9
      98.0       1.9
      99.0     100.0
     100.0      29.7
     101.0       2.3
     156.0       3.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₁₂ O₃	0.036 g : 0.5 ml CDCl₃
1,4-dioxaspiro(4.5)decan-8-one

    Assign.     Shift(ppm)

      A             4.037
      B             2.512
      C             2.019

     Hz     ppm     Int.

   1613.53   4.038   1000
   1011.47   2.531    132
   1004.39   2.514    182
    997.19   2.496    142
    812.87   2.034    152
    811.65   2.031     76
    805.54   2.016    197
    798.58   1.999    120

in CDCl3

KBr disc

nujol mull

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