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1,4-Dioxaspiro[4.5]decan-8-one

Product Name 1,4-Dioxaspiro[4.5]decan-8-one

CAS4746-97-8

MFC8H12O3

MW156.18

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  • Mass 

    MS-IW-4170          
1,4-dioxaspiro(4.5)decan-8-one
C8H12O3             (Mass of molecular ion:    156)


       Source Temperature: 240 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV


          27.0       3.1
      28.0       5.6
      29.0       1.5
      39.0       1.8
      41.0       2.0
      42.0       2.9
      43.0       3.4
      45.0       1.4
      53.0       1.1
      54.0       1.9
      55.0      13.5
      56.0       9.0
      57.0       2.2
      67.0       2.6
      71.0       1.7
      83.0       2.4
      84.0       4.0
      86.0       4.0
      97.0       2.9
      98.0       1.9
      99.0     100.0
     100.0      29.7
     101.0       2.3
     156.0       3.3

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H12 O3 0.036 g : 0.5 ml CDCl3
    1,4-dioxaspiro(4.5)decan-8-one
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             4.037
      B             2.512
      C             2.019
  

         Hz     ppm     Int.


       1613.53   4.038   1000
   1011.47   2.531    132
   1004.39   2.514    182
    997.19   2.496    142
    812.87   2.034    152
    811.65   2.031     76
    805.54   2.016    197
    798.58   1.999    120

in CDCl3



KBr disc



nujol mull





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