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MS-NW-1298 N,N-diethylacetamide C6H13NO (Mass of molecular ion: 115)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 6.5 18.0 2.4 27.0 6.4 28.0 5.6 29.0 8.3 30.0 19.0 41.0 1.7 42.0 6.6 43.0 27.6 44.0 32.9 45.0 1.0 56.0 3.0 58.0 100.0 59.0 3.7 72.0 15.1 86.0 4.0 87.0 1.2 100.0 5.9 115.0 33.5 116.0 2.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H13 N O 0.04 ml : 0.5 ml CDCl3 N,N-diethylacetamide Assign. Shift(ppm)
A 3.370 B 3.316 C 2.082 D 1.181 E 1.129 ASSIGNED BY C-H COSY.
Hz ppm Int.
313.00 3.495 39 307.44 3.433 55 305.94 3.417 125 300.38 3.354 142 298.88 3.338 137 293.25 3.275 144 291.81 3.259 56 286.19 3.196 50 186.50 2.083 1000 113.38 1.266 180 107.13 1.197 226 106.25 1.187 392 100.13 1.119 392 99.06 1.107 192 92.94 1.038 157
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