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Diethylacetamide

Product Name Diethylacetamide

CAS685-91-6

MFC6H13NO

MW115.17

¹³CNMR

Mass

MS-NW-1298          
N,N-diethylacetamide
C6H13NO             (Mass of molecular ion:    115)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       6.5
      18.0       2.4
      27.0       6.4
      28.0       5.6
      29.0       8.3
      30.0      19.0
      41.0       1.7
      42.0       6.6
      43.0      27.6
      44.0      32.9
      45.0       1.0
      56.0       3.0
      58.0     100.0
      59.0       3.7
      72.0      15.1
      86.0       4.0
      87.0       1.2
     100.0       5.9
     115.0      33.5
     116.0       2.4

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₁₃ N O	0.04 ml : 0.5 ml CDCl₃
N,N-diethylacetamide

    Assign.     Shift(ppm)

      A             3.370
      B             3.316
      C             2.082
      D             1.181
      E             1.129
     
     ASSIGNED BY C-H COSY.

     Hz     ppm     Int.

    313.00   3.495     39
    307.44   3.433     55
    305.94   3.417    125
    300.38   3.354    142
    298.88   3.338    137
    293.25   3.275    144
    291.81   3.259     56
    286.19   3.196     50
    186.50   2.083   1000
    113.38   1.266    180
    107.13   1.197    226
    106.25   1.187    392
    100.13   1.119    392
     99.06   1.107    192
     92.94   1.038    157

in CDCl3

CCl4 solution

liquid film

4880 A,200 M,liquid

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