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MS-NW-1688 adipamide C6H12N2O2 (Mass of molecular ion: 144)
Source Temperature: 190 °C Sample Temperature: 170 °C Direct, 75 eV
15.0 1.5 16.0 1.3 17.0 1.9 18.0 6.4 26.0 2.1 27.0 13.2 28.0 8.2 29.0 13.1 30.0 2.6 39.0 9.5 40.0 1.7 41.0 25.0 42.0 7.2 43.0 35.3 44.0 100.0 45.0 5.9 51.0 1.3 52.0 1.2 53.0 3.3 54.0 7.9 55.0 19.2 56.0 10.5 57.0 16.6 58.0 1.6 59.0 62.3 60.0 3.2 67.0 1.2 68.0 5.2 69.0 4.2 71.0 1.2 72.0 61.2 73.0 22.6 74.0 1.0 81.0 1.1 82.0 3.9 83.0 3.8 84.0 1.5 85.0 9.8 86.0 90.8 87.0 4.7 98.0 2.4 99.0 44.4 100.0 9.1 101.0 2.3 110.0 6.4 111.0 4.2 127.0 18.2 128.0 3.5 144.0 1.8
90 MHz in DMSO-d6
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1H NMR 89.56 MHz C6 H12 N2 O2 0.039 g : 0.5 ml DMSO-d6 adipamide Assign. Shift(ppm)
A 7.21 B 6.67 C 2.03 D 1.47
Hz ppm Int.
645.13 7.204 240 597.00 6.666 248 188.44 2.105 315 188.00 2.100 316 187.56 2.095 315 186.88 2.087 319 186.19 2.079 313 184.44 2.060 396 182.13 2.034 1000 175.63 1.962 479 172.25 1.924 163 171.19 1.912 111 139.31 1.556 151 137.06 1.531 437 133.50 1.491 534 130.13 1.453 981 126.81 1.416 454 126.31 1.411 457 123.88 1.384 251 123.50 1.379 254 122.94 1.373 260
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