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Adipic dihydrazide

Product Name Adipic dihydrazide

CAS1071-93-8

MFC6H14N4O2

MW174.2

¹³CNMR

Mass

MS-NW-0248          
adipohydrazide
C6H14N4O2           (Mass of molecular ion:    174)

   Source Temperature: 210 °C
   Sample Temperature:   0 °C
   Direct, 75 eV

      18.0       6.1
      27.0       7.0
      28.0       5.4
      29.0       7.6
      30.0       1.5
      31.0      21.0
      32.0      21.1
      33.0      13.6
      39.0       5.8
      40.0       1.0
      41.0       9.2
      42.0       2.1
      43.0       3.6
      44.0       2.0
      53.0       2.6
      54.0       1.4
      55.0      24.4
      56.0       2.5
      57.0       4.2
      59.0      21.9
      67.0       1.1
      69.0       1.6
      73.0       3.3
      74.0       3.2
      80.0       3.0
      82.0       4.4
      83.0       7.8
      84.0       1.5
      87.0       2.1
      97.0       4.8
      98.0       1.2
     101.0       3.4
     108.0       3.5
     111.0      28.1
     112.0       2.1
     114.0       2.0
     115.0      20.6
     116.0       1.4
     125.0       3.5
     142.0       1.4
     143.0     100.0
     144.0       6.6
     174.0       2.3

400 MHz in DMSO-d6

90 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₁₄ N₄ O₂	saturated in DMSO-d₆
adipohydrazide

    Assign.     Shift(ppm)

      A             8.93
      B             4.15
      C             1.991
      D             1.443

     Hz     ppm     Int.

   3569.95   8.933    562
   1658.94   4.151   1000
    801.85   2.007    432
    801.09   2.005    432
    795.75   1.992    896
    789.79   1.977    447
    577.09   1.444    914

¹H NMR	89.56 MHz
C₆ H₁₄ N₄ O₂	0.039 g : 0.5 ml DMSO-d₆
adipohydrazide

    Assign.     Shift(ppm)

      A             8.89
      B             4.14
      C             2.00
      D             1.46

     Hz     ppm     Int.

    796.56   8.895    529
    370.50   4.137   1000
    185.56   2.072    271
    185.13   2.068    270
    184.31   2.058    266
    179.38   2.003    831
    173.38   1.936    429
    170.25   1.901    150
    169.88   1.897    146
    136.69   1.527    371
    133.19   1.488    483
    130.13   1.453    813
    127.06   1.419    423
    126.81   1.416    423
    124.06   1.386    247
    123.75   1.382    248
    120.50   1.346     89

DMSO-d6

KBr disc

nujol mull

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