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MS-NW-2121 N-methyldiethylamine C5H13N (Mass of molecular ion: 87)
Source Temperature: 250 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 4.7 18.0 1.8 26.0 1.3 27.0 7.3 28.0 6.4 29.0 9.6 30.0 10.1 41.0 2.2 42.0 13.0 43.0 3.8 44.0 60.3 45.0 1.6 54.0 1.1 56.0 6.5 57.0 2.7 58.0 14.4 70.0 2.0 72.0 100.0 73.0 5.4 86.0 11.1 87.0 24.5 88.0 1.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H13 N 0.04 ml : 0.5 ml CDCl3 N-methyldiethylamine Assign. Shift(ppm)
A 2.40 B 2.204 C 1.065
Hz ppm Int.
226.81 2.533 83 226.31 2.527 85 219.25 2.449 356 212.06 2.368 400 205.19 2.292 127 197.38 2.204 1000 102.00 1.139 463 99.56 1.112 52 97.25 1.086 24 95.00 1.061 932 87.69 0.980 348
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