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MS-NW-1219 (diethylamino)acetonitrile C6H12N2 (Mass of molecular ion: 112)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 4.6 18.0 1.0 26.0 2.7 27.0 14.9 28.0 14.5 29.0 18.8 30.0 5.3 39.0 1.1 40.0 5.6 41.0 6.0 42.0 95.6 43.0 4.1 44.0 1.6 54.0 3.0 55.0 1.8 56.0 19.8 57.0 3.2 58.0 2.1 67.0 3.0 69.0 35.6 70.0 3.6 83.0 1.2 84.0 1.4 86.0 4.8 97.0 100.0 98.0 6.2 111.0 4.4 112.0 19.7 113.0 1.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H12 N2 0.04 ml : 0.5 ml CDCl3 (diethylamino)acetonitrile Assign. Shift(ppm)
A 3.602 B 2.575 C 1.101
Hz ppm Int.
322.56 3.602 736 320.06 3.574 25 242.38 2.707 104 241.94 2.702 101 234.81 2.622 425 227.69 2.543 462 222.00 2.479 34 220.88 2.467 144 105.38 1.177 504 99.81 1.115 56 98.38 1.099 1000 92.75 1.036 65 91.06 1.017 393
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