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N,N-Diethylcyanoacetamide

Product Name N,N-Diethylcyanoacetamide

CAS3010-02-4

MFC6H12N2

MW112.17

¹³CNMR

Mass

MS-NW-1219          
(diethylamino)acetonitrile
C6H12N2             (Mass of molecular ion:    112)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       4.6
      18.0       1.0
      26.0       2.7
      27.0      14.9
      28.0      14.5
      29.0      18.8
      30.0       5.3
      39.0       1.1
      40.0       5.6
      41.0       6.0
      42.0      95.6
      43.0       4.1
      44.0       1.6
      54.0       3.0
      55.0       1.8
      56.0      19.8
      57.0       3.2
      58.0       2.1
      67.0       3.0
      69.0      35.6
      70.0       3.6
      83.0       1.2
      84.0       1.4
      86.0       4.8
      97.0     100.0
      98.0       6.2
     111.0       4.4
     112.0      19.7
     113.0       1.4

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₁₂ N₂	0.04 ml : 0.5 ml CDCl₃
(diethylamino)acetonitrile

    Assign.     Shift(ppm)

      A             3.602
      B             2.575
      C             1.101

     Hz     ppm     Int.

    322.56   3.602    736
    320.06   3.574     25
    242.38   2.707    104
    241.94   2.702    101
    234.81   2.622    425
    227.69   2.543    462
    222.00   2.479     34
    220.88   2.467    144
    105.38   1.177    504
     99.81   1.115     56
     98.38   1.099   1000
     92.75   1.036     65
     91.06   1.017    393

in CDCl3

CCl4 solution

liquid film

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