9-Phenylacridine

Mass

MS-IW-7578          
9-phenylacridine
C19H13N             (Mass of molecular ion:    255)

   Source Temperature: 160 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

     100.0       2.9
     100.5       1.0
     101.0       1.2
     112.0       2.8
     112.5       2.0
     113.0       4.9
     113.5       2.2
     114.0       3.8
     125.5       1.5
     126.0      10.6
     126.5       7.3
     127.0      13.7
     127.5       9.8
     128.0       1.9
     200.0       1.3
     201.0       1.2
     202.0       1.2
     224.0       1.3
     225.0       2.2
     226.0       5.2
     227.0       3.4
     228.0       1.4
     240.0       1.1
     251.0       4.3
     252.0       7.0
     253.0      12.6
     254.0      64.3
     255.0     100.0
     256.0      19.5
     257.0       1.9

Assign. Shift(ppm) A 8.280 B 7.747 C 7.691 D 7.57 E 7.42 F 7.395 J(A,B)=8.8HZ J(A,F)=1.1HZ J(A,C)=0.7HZ J(B,C)=1.4HZ J(B,F)=6.6HZ J(C,F)=8.8HZ ASSIGNED BY C-H COSY

     Hz     ppm     Int.

   3314.58   8.294    427
   3313.84   8.292    564
   3313.48   8.291    568
   3312.74   8.290    468
   3309.20   8.281     37
   3305.79   8.272    478
   3305.05   8.270    634
   3303.96   8.268    513
   3104.86   7.769    331
   3103.39   7.766    382
   3100.83   7.759     48
   3098.27   7.753    392
   3096.80   7.749    454
   3096.07   7.747    388
   3094.60   7.744    383
   3089.48   7.731    351
   3088.13   7.728    398
   3084.47   7.718     30
   3079.71   7.707    420
   3079.10   7.705    492
   3078.37   7.703    481
   3077.76   7.702    409
   3070.92   7.685    496
   3070.31   7.683    592
   3069.58   7.681    545
   3068.97   7.680    466
   3063.48   7.666     44
   3054.57   7.644     35
   3039.18   7.605     86
   3037.48   7.601     65
   3035.77   7.597    133
   3034.30   7.593     93
   3033.08   7.590     93
   3030.64   7.584    417
   3030.15   7.583    416
   3028.56   7.579    288
   3026.61   7.574    213
   3025.15   7.570    393
   3023.19   7.565   1000
   3021.48   7.561    377
   3020.51   7.558    251
   3017.82   7.552    201
   3016.48   7.548    158
   3011.47   7.536     61
   3009.77   7.532     54
   2969.60   7.431    544
   2967.53   7.426    413
   2967.04   7.425    395
   2965.45   7.421    223
   2963.50   7.416    613
   2962.28   7.413    692
   2960.21   7.408    478
   2957.15   7.400    439
   2955.93   7.397    443
   2954.83   7.394    429
   2953.61   7.391    411
   2950.44   7.383     53
   2948.36   7.378    344
   2947.14   7.375    348