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MS-IW-8119 cis-2,6-dimethylpiperazine C6H14N2 (Mass of molecular ion: 114)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 2.4 27.0 3.9 28.0 18.4 29.0 3.1 30.0 35.7 31.0 1.6 39.0 6.5 40.0 2.3 41.0 17.3 42.0 45.5 43.0 21.5 44.0 94.5 45.0 3.6 54.0 2.4 55.0 1.3 56.0 51.1 57.0 5.3 58.0 5.6 68.0 5.6 69.0 2.3 70.0 58.9 71.0 100.0 72.0 28.0 73.0 2.3 82.0 1.5 83.0 4.1 84.0 3.6 97.0 1.3 98.0 2.0 99.0 61.8 100.0 4.0 108.0 1.4 113.0 4.9 114.0 18.9 115.0 6.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H14 N2 0.040 g : 0.5 ml CDCl3 cis-2,6-dimethylpiperazine Assign. Shift(ppm)
A 2.879 B 2.793 C 2.266 D 1.57 E 1.015
Hz ppm Int.
1158.69 2.900 125 1156.01 2.893 143 1146.24 2.869 140 1143.55 2.862 161 1132.08 2.833 34 1125.73 2.817 85 1122.92 2.810 76 1122.07 2.808 53 1119.38 2.801 102 1116.58 2.794 91 1115.60 2.792 107 1112.79 2.785 98 1109.25 2.776 97 1106.45 2.769 80 1103.03 2.760 34 916.63 2.294 176 906.37 2.268 173 904.42 2.264 177 894.29 2.238 158 628.91 1.574 86 408.94 1.024 1000 402.59 1.008 985
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