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Diethylenetriamine

Product Name Diethylenetriamine

CAS111-40-0

MFC4H13N3

MW103.17

¹³CNMR

Mass

MS-NW-8896          
bis(2-aminoethyl)amine
C4H13N3             (Mass of molecular ion:    103)

   Source Temperature: 280 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.5
      18.0      11.1
      27.0       1.8
      28.0       6.8
      29.0       2.2
      30.0      24.2
      41.0       1.8
      42.0       7.0
      43.0       5.9
      44.0     100.0
      45.0       3.4
      55.0       1.2
      56.0      10.6
      57.0       1.9
      58.0       1.4
      70.0       1.3
      71.0       1.0
      73.0      70.4
      74.0       4.1
      84.0       1.0
      86.0       3.2
      87.0       1.0
      99.0       2.5
     104.0       1.6

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₄ H₁₃ N₃	0.04 ml : 0.5 ml CDCl₃
bis(2-aminoethyl)amine

    Assign.     Shift(ppm)

      A             2.79
      B             2.69
      C             1.23

     Hz     ppm     Int.

    258.94   2.892     40
    255.75   2.856     76
    251.75   2.811     52
    250.88   2.802    171
    250.06   2.793    150
    249.25   2.784     76
    247.06   2.759    258
    246.31   2.751    297
    243.63   2.721    293
    242.81   2.712    260
    240.63   2.687     74
    239.88   2.679    147
    239.00   2.669    168
    238.19   2.660     61
    234.13   2.615     73
    231.00   2.580     40
    109.69   1.225   1000

in CDCl3

liquid film

4880 A,200 M,liquid

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