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N-(1-Naphthyl)ethylenediamine dihydrochloride

Product Name N-(1-Naphthyl)ethylenediamine dihydrochloride

CAS1465-25-4

MFC12H16Cl2N2

MW259.17

Mass

MS-NW-0643          
N-(1-naphthyl)ethylenediamine dihydrochloride
C12H14N2 2HCl       (Mass of molecular ion:    186)

   Source Temperature: 200 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      15.0       1.2
      17.0       1.7
      18.0       7.3
      28.0       5.6
      29.0       2.3
      30.0       8.3
      31.0       3.9
      32.0       2.7
      35.0       4.1
      36.0      28.5
      37.0       1.3
      38.0       8.9
      39.0       1.2
      50.0       1.2
      51.0       2.2
      63.0       2.3
      74.0       1.4
      75.0       2.3
      76.0       1.3
      77.0       4.9
      89.0       1.2
     101.0       2.5
     102.0       1.0
     115.0       5.3
     116.0       1.4
     126.0       4.2
     127.0      14.1
     128.0      18.3
     129.0      32.0
     130.0       4.0
     141.0       1.0
     143.0       2.7
     144.0       3.2
     154.0      12.3
     155.0       9.9
     156.0     100.0
     157.0      20.3
     158.0       1.7
     167.0       1.8
     168.0       1.3
     186.0      48.6
     187.0       6.7

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₂ H₁₄ N₂	0.033 g : 0.5 ml DMSO-d₆
N-(1-naphthyl)ethylenediamine dihydrochloride

    Assign.     Shift(ppm)

      A             8.50
      B             8.357
      C             7.844
      D             7.50
      E             7.49
      F             7.38
      G             7.37
      J             6.897
      K             6.62
      L             3.592
      M     *1      3.24
      N     *1      3.22

     Hz     ppm     Int.

   3396.61   8.499    286
   3348.63   8.379     32
   3345.09   8.371    220
   3341.80   8.362    128
   3337.89   8.353    212
   3335.57   8.347    234
   3331.67   8.337     36
   3140.14   7.858    241
   3137.70   7.852    246
   3134.03   7.842    149
   3131.96   7.837    200
   3130.62   7.834    290
   3127.56   7.826     40
   3007.57   7.526     63
   3005.86   7.522    104
   3000.73   7.509    289
   2999.02   7.505    279
   2997.56   7.501    316
   2994.38   7.493    567
   2991.21   7.485    302
   2989.50   7.481    253
   2987.79   7.477    264
   2982.67   7.464     98
   2980.96   7.459     67
   2959.84   7.407     73
   2951.66   7.386    498
   2948.97   7.379    399
   2946.04   7.372   1000
   2941.04   7.360     76
   2761.23   6.910    173
   2758.06   6.902    190
   2755.62   6.896    160
   2752.69   6.888    171
   2645.02   6.619    284
   1442.38   3.610    263
   1436.04   3.594    611
   1429.69   3.578    314
   1304.32   3.264     37
   1303.71   3.263     37
   1298.46   3.249    146
   1296.26   3.244    111
   1292.60   3.235    283
   1286.62   3.220    279
   1280.76   3.205    140
   1275.63   3.192     36
   1275.02   3.191     36
   1274.54   3.190     35

KBr disc

nujol mull

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