3-HYDROXY-6-METHYL-2-NITROPYRIDINE
Product Name 3-HYDROXY-6-METHYL-2-NITROPYRIDINE
CAS15128-90-2
MFC6H6N2O3
MW154.12
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MassMS-IW-0939 6-methyl-2-nitro-3-pyridinol C6H6N2O3 (Mass of molecular ion: 154)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
17.0 1.5 18.0 8.8 26.0 2.6 27.0 9.7 28.0 6.7 29.0 1.1 30.0 2.0 37.0 1.0 38.0 1.8 39.0 7.5 40.0 1.1 41.0 1.5 42.0 1.4 43.0 6.0 50.0 2.7 51.0 8.6 52.0 35.7 53.0 48.8 54.0 5.7 55.0 3.1 63.0 1.5 64.0 2.0 66.0 2.4 67.0 1.0 68.0 1.2 78.0 5.0 79.0 19.7 80.0 19.3 81.0 4.4 96.0 8.3 106.0 4.9 107.0 24.5 108.0 100.0 109.0 7.4 110.0 1.6 124.0 1.2 154.0 58.0 155.0 5.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H6 N2 O3 0.040 g : 0.5 ml CDCl3 6-methyl-2-nitro-3-pyridinol 
Assign. Shift(ppm)
A 10.13 B 7.555 C 7.501 D 2.592
Hz ppm Int.4046.94 10.127 205 3025.05 7.570 131 3016.66 7.549 263 3013.76 7.542 21 3000.95 7.509 239 2992.40 7.488 122 1036.07 2.593 1000
in CDCl3
KBr disc
nujol mull
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