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DIPHENYLIODONIUM CHLORIDE

Product Name DIPHENYLIODONIUM CHLORIDE

CAS1483-72-3

MFC12H10ClI

MW316.57

¹³CNMR

Mass

MS-NW-9113          
diphenyliodonium chloride
C12H10ClI           (Mass of molecular ion:    316)

   Source Temperature: 220 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      17.0       1.4
      18.0       7.4
      27.0       1.9
      36.0       4.2
      37.0       1.6
      38.0       4.7
      39.0       2.6
      49.0       2.0
      50.0      20.8
      51.0      32.5
      52.0       2.3
      56.0       1.6
      73.0       2.1
      74.0       7.4
      75.0       5.8
      76.0       6.3
      77.0     100.0
      78.0      10.1
     102.0       2.3
     112.0      41.2
     113.0       3.0
     114.0      14.9
     127.0       1.9
     154.0       2.2
     204.0      68.3
     205.0       4.3
     281.0       2.6

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₂ H₁₀ Cl I	0.040 g : 0.5 ml DMSO-d₆
diphenyliodonium chloride

    Assign.     Shift(ppm)

      A             8.118
      B             7.556
      C             7.438

     Hz     ppm     Int.

   3248.78   8.130    851
   3241.46   8.111    895
   3240.48   8.109    838
   3234.38   8.094     31
   3232.67   8.089     22
   3028.44   7.578    190
   3021.00   7.560    504
   3013.67   7.541    347
   2979.61   7.456    673
   2971.80   7.437   1000
   2965.94   7.422    195
   2964.23   7.418    473

in DMSO-d6

KBr disc

nujol mull

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