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MassMS-NW-3187 cyclohexene C6H10 (Mass of molecular ion: 82)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
26.0 1.9 27.0 11.8 28.0 1.3 29.0 1.8 37.0 1.0 38.0 2.3 39.0 25.8 40.0 3.7 41.0 31.9 42.0 2.7 50.0 4.3 51.0 6.2 52.0 3.1 53.0 10.5 54.0 72.3 55.0 5.4 56.0 1.3 65.0 3.4 66.0 2.2 67.0 100.0 68.0 5.7 77.0 4.6 78.0 1.3 79.0 6.7 80.0 1.0 81.0 11.2 82.0 43.7 83.0 3.1
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C6 H10 0.05 ml : 0.5 ml CDCl3 cyclohexene 
Assign. Shift(ppm)
A 5.664 B 1.991 C 1.612
Hz ppm Int.2276.86 5.698 31 2275.27 5.694 36 2273.93 5.690 39 2272.71 5.687 35 2265.50 5.669 576 2263.92 5.665 931 2262.33 5.661 534 2257.08 5.648 35 2253.78 5.640 38 2252.32 5.636 34 815.19 2.040 33 811.16 2.030 48 808.84 2.024 66 807.25 2.020 81 803.71 2.012 164 802.37 2.008 303 800.90 2.005 378 798.58 1.999 514 797.49 1.996 460 796.88 1.994 470 796.02 1.992 766 794.56 1.989 734 792.11 1.983 491 790.65 1.979 338 789.79 1.977 369 788.21 1.973 289 786.87 1.969 149 785.40 1.966 101 784.30 1.963 78 783.45 1.961 67 781.86 1.957 51 780.03 1.952 34 663.57 1.661 32 659.79 1.651 51 657.23 1.645 68 656.25 1.643 79 654.79 1.639 103 650.76 1.629 528 647.95 1.622 519 646.97 1.619 577 644.53 1.613 1000 641.85 1.607 488 640.63 1.603 475 638.06 1.597 396 634.03 1.587 74 632.45 1.583 64 629.03 1.574 32
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1H NMR 89.56 MHz C6 H10 0.05 ml : 0.5 ml CDCl3 cyclohexene Assign. Shift(ppm)
A 5.661 B 1.98 C 1.61
Hz ppm Int.508.56 5.679 540 507.06 5.662 1000 505.63 5.646 516 189.94 2.121 31 185.00 2.066 188 182.38 2.037 310 181.44 2.026 352 178.94 1.998 608 178.00 1.988 594 175.94 1.965 511 174.19 1.945 380 173.50 1.938 377 172.00 1.921 282 167.69 1.873 64 166.81 1.863 58 165.56 1.849 43 163.94 1.831 35 162.56 1.816 32 159.00 1.776 49 158.38 1.769 47 155.56 1.737 67 154.25 1.723 87 153.44 1.714 75 152.94 1.708 75 150.19 1.677 445 146.88 1.641 583 144.13 1.610 848 141.69 1.583 407 140.56 1.570 440 138.19 1.543 198 137.31 1.534 168 133.44 1.490 31 132.94 1.485 30
in CDCl3
liquid film
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