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MS-NW-9113 diphenyliodonium chloride C12H10ClI (Mass of molecular ion: 316)
Source Temperature: 220 °C Sample Temperature: 140 °C Direct, 75 eV
17.0 1.4 18.0 7.4 27.0 1.9 36.0 4.2 37.0 1.6 38.0 4.7 39.0 2.6 49.0 2.0 50.0 20.8 51.0 32.5 52.0 2.3 56.0 1.6 73.0 2.1 74.0 7.4 75.0 5.8 76.0 6.3 77.0 100.0 78.0 10.1 102.0 2.3 112.0 41.2 113.0 3.0 114.0 14.9 127.0 1.9 154.0 2.2 204.0 68.3 205.0 4.3 281.0 2.6
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C12 H10 Cl I 0.040 g : 0.5 ml DMSO-d6 diphenyliodonium chloride Assign. Shift(ppm)
A 8.118 B 7.556 C 7.438
Hz ppm Int.
3248.78 8.130 851 3241.46 8.111 895 3240.48 8.109 838 3234.38 8.094 31 3232.67 8.089 22 3028.44 7.578 190 3021.00 7.560 504 3013.67 7.541 347 2979.61 7.456 673 2971.80 7.437 1000 2965.94 7.422 195 2964.23 7.418 473
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