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WebSite > CAS DataBase List >  142246-48-8More Spectrum > 4-CHLORO-7-CHLOROSULFONYL-2,1,3-BENZOXADIAZOLE(142246-48-8)IR2

142246-48-8

4-CHLORO-7-CHLOROSULFONYL-2,1,3-BENZOXADIAZOLE

Product Name 4-CHLORO-7-CHLOROSULFONYL-2,1,3-BENZOXADIAZOLE

CAS142246-48-8

MFC6H2Cl2N2O3S

MW253.06

More

  • 142246-48-8_ms_1
    Mass

    MS-IW-7204          
    7-chloro-2,1,3-benzoxadiazole-4-sulfonyl chloride
    C6H2Cl2N2O3S        (Mass of molecular ion:    252)
    

       Source Temperature: 140 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          30.0       8.9
          36.0       1.9
          37.0       2.3
          38.0       1.3
          48.0       1.4
          49.0       1.2
          51.0       1.3
          61.0       4.8
          62.0       2.4
          63.0       1.9
          64.0       3.1
          72.0       2.5
          73.0       1.6
          74.0       3.6
          75.0       2.0
          76.0       2.3
          86.0       1.4
          87.0       5.8
          88.0      23.4
          89.0       2.8
          97.0       1.6
          98.0       5.4
         100.0       1.9
         104.0       2.2
         117.0       1.3
         122.0       1.0
         123.0       6.9
         124.0       1.8
         125.0       3.1
         139.0       2.4
         141.0       3.3
         143.0       1.5
         152.0       1.1
         153.0      13.1
         154.0       2.1
         155.0       4.3
         158.0       3.3
         160.0       2.2
         169.0       5.0
         171.0       1.7
         188.0       3.4
         190.0       2.2
         217.0     100.0
         218.0       8.2
         219.0      37.1
         220.0       3.0
         221.0       1.7
         252.0      18.1
         253.0       1.5
         254.0      12.4
         255.0       1.0
         256.0       2.4
    

400 MHz in CDCl3

  • 142246-48-8_1hnmr_0

    1H NMR 399.65 MHz
    C6 H2 Cl2 N2 O3 S 0.040 g : 0.5 ml CDCl3
    7-chloro-2,1,3-benzoxadiazole-4-sulfonyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.202 B 7.691

         Hz     ppm     Int.
    

       3281.86   8.212    905
       3279.05   8.205     29
       3277.22   8.201     31
       3274.29   8.193   1000
       3081.67   7.711     23
       3077.39   7.701    960
       3074.71   7.694     30
       3074.10   7.692     34
       3073.12   7.690     34
       3069.82   7.682    916
    

in CDCl3

  • 142246-48-8_13cnmr_0

KBr disc

  • 142246-48-8_ir1_2

nujol mull

  • 142246-48-8_ir2_1