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N,N-DIMETHYL-M-TOLUIDINE

Product Name N,N-DIMETHYL-M-TOLUIDINE

CAS121-72-2

MFC9H13N

MW135.21

¹³CNMR

Mass

MS-NW-0585          
N,N-dimethyl-m-toluidine
C9H13N              (Mass of molecular ion:    135)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       2.0
      27.0       1.3
      39.0       4.5
      41.0       1.5
      42.0       5.0
      44.0       2.2
      50.0       1.2
      51.0       3.1
      52.0       1.3
      58.5       1.0
      63.0       2.8
      64.0       1.0
      65.0       7.1
      66.5       4.6
      67.5       2.0
      77.0       4.8
      78.0       1.7
      79.0       1.5
      89.0       2.0
      90.0       1.2
      91.0      15.6
      92.0       3.4
      93.0       1.9
     104.0       1.0
     105.0       2.1
     106.0       1.3
     118.0       8.3
     119.0      10.3
     120.0       6.2
     121.0       1.9
     132.0       1.3
     133.0       1.1
     134.0     100.0
     135.0      82.5
     136.0       8.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₉ H₁₃ N	10.7 mol% in CDCl₃
N,N-dimethyl-m-toluidine

    Assign.     Shift(ppm)

      A          6.46 to 6.62
      B             7.088
      C             2.88
      D             2.30

     Hz     ppm     Int.

    635.88   7.101     31
    628.75   7.021     37
    589.44   6.582    122
    588.94   6.576    113
    586.69   6.551     37
    585.94   6.543     36
    585.19   6.535     31
    583.00   6.510     66
    258.06   2.882   1000
    255.75   2.856     54
    206.31   2.304    274
    205.69   2.297    256

in CDCl3

CCl4 solution

liquid film

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