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N,N-Dimethylcyclohexylamine

Product Name N,N-Dimethylcyclohexylamine

CAS98-94-2

MFC8H17N

MW127.23

¹³CNMR

Mass

MS-NW-0571          
N,N-dimethylcyclohexylamine
C8H17N              (Mass of molecular ion:    127)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       1.5
      27.0       2.4
      28.0       1.1
      29.0       1.7
      39.0       2.7
      41.0       4.5
      42.0       8.8
      43.0       2.2
      44.0       6.3
      45.0       1.0
      53.0       1.0
      55.0       3.4
      56.0       5.4
      58.0       6.2
      68.0       1.0
      70.0       4.1
      71.0      19.2
      72.0       1.2
      82.0       1.3
      84.0     100.0
      85.0       7.4
      98.0       2.9
     126.0       2.0
     127.0      17.7
     128.0       1.6

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₁₇ N	0.05 ml : 0.5 ml CDCl₃
N,N-dimethylcyclohexylamine

    Assign.     Shift(ppm)

      A             2.266
      B             2.128
      C             1.850
      D             1.783
      E             1.618
      F             1.22
      G             1.18
      J             1.12
     
     ASSIGNED BY C-H COSY.

     Hz     ppm     Int.

    905.76   2.267   1000
    854.25   2.138     43
    850.95   2.130     64
    745.61   1.866     80
    744.51   1.863     82
    739.50   1.851     51
    737.79   1.847     49
    734.38   1.838     72
    733.15   1.835     77
    721.19   1.805     52
    717.90   1.797     64
    714.36   1.788     53
    713.13   1.785     48
    711.67   1.781     46
    708.50   1.773     68
    707.89   1.772     69
    705.57   1.766     91
    652.34   1.633     43
    640.01   1.602     44
    504.76   1.264     42
    501.71   1.256     56
    492.31   1.232     61
    489.38   1.225     87
    486.82   1.219     63
    481.08   1.204     94
    480.83   1.204     94
    480.22   1.202     94
    477.78   1.196     68
    472.78   1.183    103
    472.17   1.182    103
    462.16   1.157     66
    459.72   1.151     87
    447.39   1.120     60

in CDCl3

liquid film

4880 A,200 M,liquid

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