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MS-NW-0586 N,N-dimethyl-o-toluidine C9H13N (Mass of molecular ion: 135)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 3.2 27.0 2.4 28.0 1.7 38.0 1.3 39.0 8.4 41.0 2.7 42.0 8.1 43.0 1.0 44.0 11.0 50.0 2.2 51.0 6.0 52.0 2.6 53.0 1.5 58.5 1.4 62.0 1.3 63.0 4.7 64.0 1.5 65.0 15.4 65.5 1.0 66.0 2.0 66.5 4.9 67.0 1.3 67.5 1.6 77.0 8.4 78.0 3.3 79.0 2.2 89.0 3.1 90.0 1.8 91.0 30.6 92.0 5.4 93.0 3.3 103.0 1.1 104.0 16.5 105.0 5.0 106.0 2.8 117.0 3.8 118.0 22.1 119.0 9.1 120.0 69.3 121.0 7.8 132.0 3.3 134.0 82.3 135.0 100.0 136.0 9.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H13 N 0.05 ml : 0.5 ml CDCl3 N,N-dimethyl-o-toluidine Assign. Shift(ppm)
A 7.14 B 7.13 C 7.008 D 6.925 E 2.667 F 2.315
Hz ppm Int.
2856.57 7.148 70 2855.96 7.147 100 2855.35 7.145 82 2854.25 7.142 61 2853.52 7.141 54 2849.49 7.130 106 2849.00 7.129 106 2848.39 7.128 120 2847.78 7.126 110 2846.80 7.124 79 2846.07 7.122 64 2842.65 7.113 53 2842.04 7.112 55 2841.55 7.111 39 2840.94 7.109 35 2840.33 7.108 30 2804.57 7.018 82 2803.59 7.016 85 2796.26 6.997 57 2794.92 6.994 54 2775.02 6.944 53 2774.05 6.942 49 2767.82 6.926 72 2766.60 6.923 80 2760.62 6.908 36 2760.25 6.907 36 2759.28 6.905 36 1065.92 2.668 1000 925.05 2.315 490
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