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MS-NW-5568 ((1-naphthyl)methyl)amine C11H11N (Mass of molecular ion: 157)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 1.7 28.0 7.1 29.0 1.7 30.0 15.6 39.0 2.7 50.0 3.0 51.0 5.0 52.0 1.2 62.0 1.9 63.0 5.0 64.0 2.1 65.0 2.7 74.0 3.1 75.0 3.8 76.0 2.6 76.5 2.2 77.0 8.1 77.5 4.8 78.0 4.5 78.5 3.5 86.0 1.0 87.0 1.5 89.0 1.9 91.0 1.0 98.0 1.1 101.0 2.7 102.0 3.0 103.0 1.0 113.0 1.0 115.0 9.0 116.0 1.1 126.0 5.1 127.0 16.6 128.0 31.0 129.0 41.6 130.0 5.9 139.0 7.7 140.0 4.8 141.0 19.6 142.0 3.4 153.0 3.8 154.0 7.0 155.0 2.7 156.0 100.0 157.0 93.8 158.0 11.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H11 N 0.05 ml : 0.5 ml CDCl3 ((1-naphthyl)methyl)amine Assign. Shift(ppm)
A 7.945 B 7.79 C 7.679 D *1 7.45 E *1 7.41 F 7.35 G 7.34 J 4.168 K 1.77
Hz ppm Int.
3180.66 7.959 192 3179.44 7.956 218 3178.59 7.954 203 3173.71 7.942 108 3172.61 7.939 185 3171.63 7.937 236 3171.02 7.935 238 3122.92 7.815 30 3118.04 7.802 225 3117.07 7.800 209 3115.72 7.797 187 3114.01 7.792 107 3113.40 7.791 110 3110.35 7.783 291 3108.52 7.779 266 3105.22 7.770 63 3101.68 7.761 30 3073.12 7.690 170 3070.31 7.683 185 3066.53 7.674 151 3063.72 7.667 199 2991.09 7.485 30 2990.23 7.483 31 2989.62 7.481 32 2988.65 7.479 34 2988.28 7.478 34 2986.57 7.473 62 2985.23 7.470 148 2983.64 7.466 178 2981.93 7.462 81 2978.52 7.453 312 2976.81 7.449 294 2975.46 7.446 181 2970.83 7.434 536 2968.87 7.429 502 2966.43 7.423 143 2964.11 7.417 177 2963.01 7.415 274 2961.55 7.411 300 2959.35 7.405 112 2958.01 7.402 119 2956.18 7.397 169 2954.71 7.394 131 2952.76 7.389 48 2951.90 7.387 47 2951.66 7.386 47 2950.81 7.384 47 2950.32 7.383 46 2949.95 7.382 46 2949.46 7.381 45 2948.73 7.379 46 2948.36 7.378 45 2948.12 7.377 45 2946.04 7.372 153 2938.96 7.354 498 2934.94 7.344 374 2932.25 7.338 1000 2927.98 7.327 122 1665.77 4.169 623 1653.44 4.138 33 1652.83 4.136 33 1652.47 4.135 33 707.89 1.772 181
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