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2,6-Diacetylpyridine

Product Name 2,6-Diacetylpyridine

CAS1129-30-2

MFC9H9NO2

MW163.17

¹³CNMR

Mass

MS-NW-6519          
2,6-diacetylpyridine
C9H9NO2             (Mass of molecular ion:    163)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       7.1
      26.0       1.3
      27.0       1.4
      28.0       1.9
      37.0       1.0
      38.0       1.8
      39.0       3.3
      42.0       3.7
      43.0     100.0
      44.0       2.5
      50.0       4.9
      51.0       6.2
      52.0       3.5
      53.0       1.0
      63.0       1.7
      64.0       1.8
      65.0       3.2
      66.0       2.3
      75.0       1.3
      76.0       2.8
      77.0       3.2
      78.0       9.1
      79.0       8.7
      92.0       1.8
      93.0      20.4
      94.0       1.6
     106.0      24.6
     107.0       1.8
     120.0      27.7
     121.0      36.7
     122.0       3.5
     135.0      19.2
     136.0       1.8
     148.0       1.9
     163.0      58.8
     164.0       6.3

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₉ H₉ N O₂	0.046 g : 0.5 ml CDCl₃
2,6-diacetylpyridine

    Assign.     Shift(ppm)

      A             8.22
      B             8.00
      C             2.799

     Hz     ppm     Int.

    741.25   8.277     46
    738.94   8.251     63
    732.94   8.184    139
    732.50   8.179    125
    722.50   8.068     80
    716.50   8.001     44
    713.50   7.967     27
    250.50   2.798   1000

in CDCl3

KBr disc

nujol mull

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