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2-CYANOETHYLTRICHLOROSILANE

Product Name 2-CYANOETHYLTRICHLOROSILANE

CAS1071-22-3

MFC3H4Cl3NSi

MW188.52

¹³CNMR

Mass

MS-IW-8616          
3-(trichlorosilyl)propionitrile
C3H4Cl3NSi          (Mass of molecular ion:    187)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      26.0       1.8
      27.0       3.4
      28.0       9.8
      36.0       3.2
      38.0       1.1
      49.0       1.9
      51.0       1.4
      52.0       2.3
      53.0       1.4
      54.0       9.7
      58.0       3.6
      63.0      20.2
      64.0       1.5
      65.0       7.5
      86.0       1.4
      98.0      14.6
      99.0       3.3
     100.0      10.0
     101.0       2.1
     102.0       2.0
     112.0       1.0
     124.0       6.2
     125.0       1.7
     126.0       4.3
     133.0      97.4
     134.0       5.1
     135.0      98.1
     136.0       4.9
     137.0      34.0
     138.0       1.6
     139.0       4.4
     147.0       2.2
     149.0       2.3
     151.0       1.9
     152.0       2.8
     153.0       1.2
     154.0       1.9
     160.0       6.0
     162.0       5.8
     164.0       2.0
     186.0      99.4
     187.0       9.5
     188.0     100.0
     189.0       9.1
     190.0      34.5
     191.0       3.1
     192.0       4.5
     266.0       1.3
     268.0       1.8
     270.0       1.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₃ H₄ Cl₃ N Si	0.048 g : 0.5 ml CDCl₃
3-(trichlorosilyl)propionitrile

    Assign.     Shift(ppm)

      A             2.626
      B             1.823

     Hz     ppm     Int.

   1061.89   2.658     51
   1058.11   2.648    856
   1053.10   2.636    242
   1051.15   2.631    520
   1050.05   2.628    913
   1048.34   2.624    425
   1046.51   2.619    238
   1041.87   2.607   1000
    741.21   1.855     43
    736.57   1.844    950
    731.81   1.832    239
    729.86   1.827    447
    728.39   1.823    867
    727.05   1.820    449
    725.22   1.815    213
    723.63   1.811     57
    720.34   1.803    856
    715.58   1.791     29

in CDCl3

KBr disc

nujol mull

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