3-Cyanopyridine

Mass

MS-NW-8720          
nicotinonitrile
C6H4N2              (Mass of molecular ion:    104)

   Source Temperature: 260 °C
   Sample Temperature: 140 °C
   Reservoir, 75 eV

      26.0       6.6
      28.0       2.7
      37.0       2.6
      38.0       3.1
      39.0       1.7
      49.0       3.4
      50.0      21.6
      51.0      12.6
      52.0       5.4
      53.0       4.3
      64.0       3.7
      74.0       1.0
      75.0       8.0
      76.0      17.1
      77.0      55.8
      78.0       5.1
     103.0       3.3
     104.0     100.0
     105.0       7.6

Parameter ppm Hz D(A) 9.22 D(B) 8.47 D(C) 7.81 D(D) 9.03 J(A,B) 2.1 J(A,C) 1.0 J(A,D) 0.3 J(B,C) 8.1 J(B,D) 1.6 J(C,D) 5.0 BRUEGEL,W. Z.ELEKTROCHEM.(BER.BUNSENGES.PHYS.CHEM.) 66, 159 (1962) J(A,D) LESS THAN 0.3HZ.

     Hz     ppm     Int.

   2767.43   9.225    896
   2766.57   9.222    992
   2765.45   9.218   1000
   2764.57   9.215    914
   2712.31   9.041    736
   2710.75   9.036    759
   2707.31   9.024    766
   2705.75   9.019    772
   2546.96   8.490    420
   2545.14   8.484    619
   2543.30   8.478    414
   2538.86   8.463    462
   2537.04   8.457    671
   2535.21   8.451    441
   2349.91   7.833    478
   2349.00   7.830    480
   2344.91   7.816    483
   2343.99   7.813    492
   2341.82   7.806    470
   2340.90   7.803    458
   2336.81   7.789    434
   2335.91   7.786    430