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Ferric acetylacetonate

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Ferric acetylacetonate Basic information
Ferric acetylacetonate Chemical Properties
  • Melting point:180-182 °C (dec.)(lit.)
  • Boiling point:110°C 2mm
  • Density 5.24 g/mL at 25 °C(lit.)
  • vapor pressure 2.6 hPa (110 °C)
  • storage temp. Store below +30°C.
  • solubility Soluble in toluene.
  • form Powder
  • Specific Gravity5.24
  • color Red
  • Water Solubility 2 g/L (20 ºC)
  • Hydrolytic Sensitivity4: no reaction with water under neutral conditions
  • BRN 4157960
  • Stability:Stable. Incompatible with strong bases, strong oxidizing agents.
  • NIST Chemistry ReferenceIron tris(acetylacetonate)(14024-18-1)
  • EPA Substance Registry SystemIron, tris(2,4-pentanedionato-.kappa.O,.kappa.O')-, (OC-6-11)- (14024-18-1)
Safety Information
  • Hazard Codes Xn
  • Risk Statements 22-36
  • Safety Statements 26-37/39
  • WGK Germany 3
  • RTECS NO8960000
  • 21
  • TSCA Yes
  • HS Code 29420000
  • ToxicityLD50 orally in Rabbit: 1872 mg/kg
MSDS
Ferric acetylacetonate Usage And Synthesis
  • Chemical Propertiesdark red powder
  • UsesModerating and combustion catalyst, solid fuel catalyst, bonding agent, curing accelerator, intermediate.
  • PreparationFerric acetylacetonate is prepared by shaking ferric hydroxide with an alcoholic solution of the reagent. It is an excellent quencher of triplet states.
  • Purification MethodsWhen recrystallised twice from *benzene/pet ether, it has m 181.3-182.3o corr [Finn et al. J Chem Soc 1256 1938]. However, when recrystallised from EtOH or Et2O it has m 179o [Hantzsch & Desch Justus Liebigs Ann Chem 323 13 1902]. Recrystallisation from absolute EtOH gives material with m 159.5o [Emmert & Jacob Chem Ber 67 286 1934]. Dry it for 1hour at 120o. [Beilstein 1 IV 606, 2 IV 1908.]
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