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3'-Hydroxypropiophenone

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3'-Hydroxypropiophenone Basic information
3'-Hydroxypropiophenone Chemical Properties
  • Melting point:82 °C
  • Boiling point:288.9±23.0 °C(Predicted)
  • Density 1.104±0.06 g/cm3(Predicted)
  • pka9.09±0.10(Predicted)
  • CAS DataBase Reference13103-80-5(CAS DataBase Reference)
Safety Information
3'-Hydroxypropiophenone Usage And Synthesis
  • PreparationPreparation by diazotization of m-aminopropiophenone, followed by decomposition of the diazonium salt obtained, (71%)
    Also obtained by saponification of 3-acetoxypropiophenone (b.p.2 127–128°) with refluxing 10% sodium hydroxide for 2–3 h (83%)
    Also obtained by reductive deamination of 2-amino-5-hydroxypropiophenone (diazotization, followed by decomposition of the diazonium salt formed with copper powder in ethanol)
    Also obtained by reaction of ethylmagnesium bromide with 3-hydroxy-N, N-diethylbenzamide in refluxing n-butyl ether for 4 h (75%)
    Also obtained by treatment of 3-methoxypropiophenone (b.p.0.05 70–76°) with pyridinium chloride at 210° for 30 min (85%)
    Also obtained by treatment of 1-hydroxy-1-(3-hydroxyphenyl)propane (m.p. 105–107°) with DDQ in dioxane for 72 h (97%).
3'-Hydroxypropiophenone(13103-80-5)Related Product Information
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