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Dibenzylamine

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Dibenzylamine Basic information
Dibenzylamine Chemical Properties
  • Melting point:-26 °C (lit.)
  • Boiling point:300 °C (lit.)
  • Density 1.026 g/mL at 25 °C (lit.)
  • refractive index n20/D 1.574(lit.)
  • Flash point:290 °F
  • storage temp. Keep in dark place,Inert atmosphere,Room temperature
  • solubility 0.4g/l
  • form Liquid
  • pkapK1:8.52(+1) (25°C)
  • color Clear colorless to light yellow
  • PH8.9 (H2O, 20℃)
  • Water Solubility 0.05 g/L (20 ºC)
  • Merck 14,3011
  • BRN 909664
  • Stability:Stable. Incompatible with oxidizing agents, acid anhydrides, acids, acid chlorides, chloroformates.
  • InChIKeyBWLUMTFWVZZZND-UHFFFAOYSA-N
  • CAS DataBase Reference103-49-1(CAS DataBase Reference)
  • NIST Chemistry ReferenceDibenzylamine(103-49-1)
  • EPA Substance Registry SystemDibenzylamine (103-49-1)
Safety Information
  • Hazard Codes Xn,Xi,C
  • Risk Statements 22-36/38-52/53-34
  • Safety Statements 26-61-45-36/37/39
  • RIDADR 2810
  • WGK Germany 3
  • Hazard Note Irritant/Corrosive
  • TSCA Yes
  • HazardClass 8
  • PackingGroup III
  • HS Code 29214980
MSDS
Dibenzylamine Usage And Synthesis
  • Chemical PropertiesColorless to light yellow liqui
  • UsesDetection of cobalt, cyanate and iron.
  • Synthesis Reference(s)Tetrahedron Letters, 26, p. 4633, 1985 DOI: 10.1016/S0040-4039(00)98771-9
    The Journal of Organic Chemistry, 60, p. 5969, 1995 DOI: 10.1021/jo00123a041
  • Purification MethodsPurify the amine by distillation in a vacuum. It causes burns to the skin. The dihydrochloride has m 265-266o (from MeOH/HCl), and the tetraphenyl boronate has m 129-133o. [Bradley & Maisey J Chem Soc 247 1954, Hall J Phys Chem 60 63 1956, Donetti & Bellora J Org Chem 37 3352 1972, Beilstein 12 IV 2179.]
Dibenzylamine Preparation Products And Raw materials
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