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1-IODOADAMANTANE

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1-IODOADAMANTANE Basic information
1-IODOADAMANTANE Chemical Properties
  • Melting point:75-76 °C(lit.)
  • Boiling point:265.7±9.0℃ (760 Torr)
  • Density 1.63±0.1 g/cm3 (20 ºC 760 Torr)
  • refractive index 1.6610 (estimate)
  • Flash point:115.9±13.1℃
  • Stability:Stable, but light and moisture sensitive. Incompatible with strong oxidizing agents.
Safety Information
  • WGK Germany 3
MSDS
1-IODOADAMANTANE Usage And Synthesis
  • Chemical Propertiessolid
  • Synthesis Reference(s)The Journal of Organic Chemistry, 48, p. 2766, 1983 DOI: 10.1021/jo00164a026
  • Purification MethodsDissolve the iodide in Et2O, shake with aqueous NaHSO3, aqueous K2CO3, and H2O, dry (Na2SO4), evaporate and recrystallise it from MeOH at -70o (to avoid alcoholysis) to give white crystals. [Schleyer & Nicholas J Am Chem Soc 83 2700 1961, lit m of 151-152.5o is incorrect.] Also purify by recrystallisation from pet ether (40-60oC) followed by rigorous drying and repeated sublimation. [Beilstein 5 IV 470.]
1-IODOADAMANTANE(768-93-4)Related Product Information
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