122-19-0

White solid or thick liquid with a mild odor.

Acidic organic salt solutions contain moderate concentrations of hydrogen ions and have pH's of less than 7.0. They react as acids to neutralize bases.

Insoluble in water.

Ingestion causes gastrointestinal disturbances. Contact with chemical irritates eyes and skin and may damage eyes.

Special Hazards of Combustion Products: Toxic oxides of nitrogen and hydrochloric acid fumes may form in fires.

Paste

Synthesis of benzyldimethylstearylammonium chloride: put 450kg of dimethyl octadecylamine into the reaction kettle, heat to 80~85℃, and slowly add 180kg of benzyl chloride under stirring in 1.5~2h. Keep warm at 80～90℃ during the drop addition. After the dosing is completed, increase the temperature to 100~105℃, hold the reaction for several hours and take samples to measure the pH value. When the pH value of 1% aqueous solution reaches 6~6.5, the reaction is completed. Cool down to 60℃ and discharge to get benzyldimethylstearylammonium chloride.

Notclassified

Store at -20°C

Crystallise the salt from acetone, EtOAc or EtOAc/ Et2O. [Sumiki et al. J Agric Chem Soc Jpn 26 325 1952, Chem Abstr 3505 1953, Beilstein 12 III 2212, 12 IV 2168.]