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MS-NW-0584 N,N-dimethyl-p-toluidine C9H13N (Mass of molecular ion: 135)
Source Temperature: 280 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 2.0 27.0 1.4 39.0 4.5 41.0 1.8 42.0 4.6 44.0 1.7 50.0 1.5 51.0 3.4 52.0 1.6 63.0 2.7 65.0 7.5 66.0 1.1 66.5 3.0 67.0 1.0 67.5 2.5 77.0 4.6 78.0 1.9 79.0 1.3 89.0 1.9 90.0 1.5 91.0 17.8 92.0 3.3 93.0 1.5 104.0 1.0 105.0 1.6 106.0 1.0 117.0 1.1 118.0 11.2 119.0 13.2 120.0 6.4 121.0 1.3 132.0 1.4 133.0 1.3 134.0 100.0 135.0 76.2 136.0 7.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H13 N 0.05 ml : 0.5 ml CDCl3 N,N-dimethyl-p-toluidine Assign. Shift(ppm)
A 7.02 B 6.665 C 2.856 D 2.238
Hz ppm Int.
634.69 7.087 65 634.00 7.080 60 633.25 7.071 37 632.44 7.062 28 631.75 7.054 24 628.13 7.014 35 627.50 7.007 38 626.44 6.995 60 625.81 6.988 96 625.19 6.981 84 602.88 6.732 21 600.25 6.703 115 598.00 6.678 36 593.69 6.629 31 591.50 6.605 68 255.88 2.858 1000 200.50 2.239 280
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