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MassMS-NW-1783 5-nitro-o-toluidine C7H8N2O2 (Mass of molecular ion: 152)
Source Temperature: 240 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 2.9 26.0 1.1 27.0 5.9 28.0 8.4 29.0 1.2 30.0 3.5 37.0 2.1 38.0 5.0 39.0 15.6 40.0 2.4 41.0 5.6 42.0 5.3 44.0 1.8 46.0 1.1 50.0 8.3 51.0 18.5 52.0 15.2 53.0 13.3 54.0 7.1 55.0 1.2 61.0 1.1 62.0 3.3 63.0 8.0 64.0 2.7 65.0 7.8 66.0 7.3 67.0 4.0 68.0 1.0 74.0 2.7 75.0 2.4 76.0 3.4 77.0 73.4 78.0 18.0 79.0 62.8 80.0 7.6 89.0 2.5 91.0 4.6 92.0 1.5 93.0 5.7 94.0 15.0 95.0 1.3 104.0 13.1 105.0 7.0 106.0 84.2 107.0 7.9 122.0 4.7 136.0 1.2 152.0 100.0 153.0 9.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H8 N2 O2 0.044 g : 0.5 ml CDCl3 5-nitro-o-toluidine 
Assign. Shift(ppm)
A 7.52 B 7.47 C 7.14 D 3.93 E 2.218
Hz ppm Int.678.38 7.575 61 676.13 7.550 112 669.13 7.472 495 642.88 7.179 139 642.38 7.173 138 633.75 7.077 94 351.88 3.929 76 198.69 2.219 1000
in CDCl3
CCl4 solution
KBr disc
nujol mull
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