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MassMS-NW-0571 N,N-dimethylcyclohexylamine C8H17N (Mass of molecular ion: 127)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.5 27.0 2.4 28.0 1.1 29.0 1.7 39.0 2.7 41.0 4.5 42.0 8.8 43.0 2.2 44.0 6.3 45.0 1.0 53.0 1.0 55.0 3.4 56.0 5.4 58.0 6.2 68.0 1.0 70.0 4.1 71.0 19.2 72.0 1.2 82.0 1.3 84.0 100.0 85.0 7.4 98.0 2.9 126.0 2.0 127.0 17.7 128.0 1.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H17 N 0.05 ml : 0.5 ml CDCl3 N,N-dimethylcyclohexylamine 
Assign. Shift(ppm)
A 2.266 B 2.128 C 1.850 D 1.783 E 1.618 F 1.22 G 1.18 J 1.12 ASSIGNED BY C-H COSY.
Hz ppm Int.905.76 2.267 1000 854.25 2.138 43 850.95 2.130 64 745.61 1.866 80 744.51 1.863 82 739.50 1.851 51 737.79 1.847 49 734.38 1.838 72 733.15 1.835 77 721.19 1.805 52 717.90 1.797 64 714.36 1.788 53 713.13 1.785 48 711.67 1.781 46 708.50 1.773 68 707.89 1.772 69 705.57 1.766 91 652.34 1.633 43 640.01 1.602 44 504.76 1.264 42 501.71 1.256 56 492.31 1.232 61 489.38 1.225 87 486.82 1.219 63 481.08 1.204 94 480.83 1.204 94 480.22 1.202 94 477.78 1.196 68 472.78 1.183 103 472.17 1.182 103 462.16 1.157 66 459.72 1.151 87 447.39 1.120 60
in CDCl3
liquid film
4880 A,200 M,liquid
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